Appendix E Groundwater Well Construction and Development Logs, Sampling Logs, and Laboratory Analytical Reports ANALYTICAL REPORT Job Number: 660-27893-1 Job Description: Raytheon For: ARCADIS U.S., Inc. 14055 Riveredge Drive Suite 400 Tampa, FL 33637 Attention: Mr. Gus Suarez _____________________________________________ Approved for release. Nancy Robertson Project Manager II 4/6/2009 2:17 PM Designee for Natalie Tafuni Project Manager I [email protected] 04/06/2009 Revision: 1 cc: Ms. Jane Kennedy Mr. Melvin Rivera Albert Zumbuhl Methods: FDEP, DOH Certification #: TestAmerica Tampa E84282 TestAmerica Tallahassee E81005 These test results meet all the requirements of NELAC unless specified in the case narrative. All questions regarding this test report should be directed to the TestAmerica Project Manager who signed this test report. The estimated uncertainty associated with these reported results is available upon request. The results contained in this test report relate only to these samples included herein. TestAmerica Laboratories, Inc. TestAmerica Tampa 6712 Benjamin Road, Suite 100, Tampa, FL 33634 Tel (813) 885-7427 Fax (813) 885-7049 www.testamericainc.com Page 1 of 221 04/06/2009 Job Narrative 660-J27893-1 Comments No additional comments. Receipt All samples were received in good condition within temperature requirements. 8260B The batch sample duplicate(job 660-27916) %RPD for batch 660-75683 has a result of NC for all analytes. The sample result and the sample duplicate result are both Non-detect for these compounds. The Laboratory LIMs system flags the %RPD in this scenario as NC, or "not calculated". This report was revised on 4/6/09. A peak was misidentified as Chloroethane for sample DMW-N_022509. Upon review of the data, per client request, it was noticed this was matrix interference causing background noise. This revised report has the corrected results for this sample. 6010B The matrix spike / matrix spike duplicate (MS/MSD) recoveries for batch 660-75517 were outside of control limits for calcium and iron. The spike concentration of 1.0 mg/l is significantly less than 4X the sample concentration for Calcium. Therefore, the MS/MSD recovery calculations are not applicable. The associated laboratory control standard (LCS) met acceptance criteria. The data are flagged with J3 qualifiers. 353.2 The matrix spike duplicate (MSD) recovery for batch 660-75644 was outside of control limits for NOX. The associated laboratory control standard (LCS) and matrix spike (MS) met acceptance criteria. The data are flagged with J3 qualifiers. 2320B The sample duplicate %RPD for batch 660-75553 has a result of NC for alkalinity. The sample result and the sample duplicate result are both Non-detect for this compound. The Laboratory LIMs system flags the %RPD in this scenario as NC, or "not calculated". The sample duplicate %RPD for batch 660-75622 has a result of NC for alkalinity. The sample result and the sample duplicate result are both Non-detect for this compound. The Laboratory LIMs system flags the %RPD in this scenario as NC, or "not calculated". 300.0 The matrix spike / matrix spike duplicate (MS/MSD) recoveries for batch 660-75752 were outside of control limits for chloride and sulfate only, possibly due to matrix interference from sample. The associated laboratory control standard (LCS) met acceptance criteria. The data are flagged with J3 qualifiers. Page 2 of 221 04/06/2009 EXECUTIVE SUMMARY - Detections Client: ARCADIS U.S., Inc. Lab Sample ID Analyte 660-27893-1 Client Sample ID Result / Qualifier Chloromethane 20 ug/L 8260B 16 1.0 ug/L 8260C SIM/ID 5.2 1.0 ug/L 8260C SIM/ID 4.3 78 1.0 1.0 ug/L ug/L 8260B 8260C SIM/ID 1.9 20 1.0 1.0 ug/L ug/L 8260B 8260C SIM/ID 9.5 1.0 ug/L 8260C SIM/ID 1.4 1.0 ug/L 8260C SIM/ID SMW-H_022509 1,4-Dioxane 660-27893-14 45 SMW-E_022509 1,4-Dioxane 660-27893-13 8260B IDPT-9_022509 1,4-Dioxane 660-27893-12 ug/L IDPT-8_022509 1,1-Dichloroethane 1,4-Dioxane 660-27893-11 1.0 IDPT-15_022509 1,1-Dichloroethane 1,4-Dioxane 660-27893-10 2.8 IMW-D_022509 1,4-Dioxane 660-27893-7 Method DMW-C_022509 1,4-Dioxane 660-27893-5 Units DMW-Q_022509 Acetone 660-27893-4 Reporting Limit DMW-P_022509 Chloroform 660-27893-3 Job Number: 660-27893-1 0.80 I 1.0 ug/L 8260C SIM/ID 1.1 I 4.0 ug/L 8260B DMW-N_022509 TestAmerica Tampa Page 3 of 221 04/06/2009 EXECUTIVE SUMMARY - Detections Client: ARCADIS U.S., Inc. Lab Sample ID Analyte 660-27893-17 Client Sample ID Result / Qualifier ug/L 8260C SIM/ID 27 1.0 ug/L 8260C SIM/ID 1300 40 ug/L 8260B 0.83 I 1.0 ug/L 8260B 1.1 0.51 14 I 1.0 1.0 1.0 ug/L ug/L ug/L 8260B 8260B 8260C SIM/ID 1.0 2.0 ug/L ug/L 8260B 8260B 1.0 ug/L 8260C SIM/ID 1.0 1.0 1.0 5.0 5.0 ug/L ug/L ug/L ug/L ug/L 8260B 8260B 8260B 8260B 8260C SIM/ID IDPT-1_022509 IDPT-2_022509 13 1.8 I IDPT-5_022509 1,4-Dioxane 660-27893-29 1.0 I H-1_022509 Toluene m-Xylene & p-Xylene 660-27893-28 8260B 8260C SIM/ID IMW-J_022509 1,1-Dichloroethane Vinyl chloride 1,4-Dioxane 660-27893-27 ug/L ug/L IDPT-12_022509 Benzene 660-27893-26 40 1.0 0.95 Acetone 660-27893-23 Method SMW-N_022509 1,4-Dioxane 660-27893-20 Units 920 5.1 1,4-Dioxane 660-27893-19 Reporting Limit DMW-I_022509 Acetone 1,4-Dioxane 660-27893-18 Job Number: 660-27893-1 24 IDPT-6_022509 1,1-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene Vinyl chloride 1,4-Dioxane 16 0.59 4.0 330 100 I TestAmerica Tampa Page 4 of 221 04/06/2009 EXECUTIVE SUMMARY - Detections Client: ARCADIS U.S., Inc. Lab Sample ID Analyte 660-27893-30 Client Sample ID Result / Qualifier 1,4-Dioxane 1.0 ug/L 8260C SIM/ID 470 3800 160 50 50 50 ug/L ug/L ug/L 8260B 8260B 8260C SIM/ID 160 1.0 7.9 20 1.0 1.0 ug/L ug/L ug/L 8260B 8260B 8260C SIM/ID 3.4 110 2.0 2.0 ug/L ug/L 8260B 8260C SIM/ID 36 14 2.7 1.5 6.2 1.0 1.0 1.0 1.0 1.0 ug/L ug/L ug/L ug/L ug/L 8260B 8260B 8260B 8260B 8260C SIM/ID 9800 55 400 20 ug/L ug/L 8260B 8260C SIM/ID 88 2.0 ug/L 8260C SIM/ID I DMW-F_022509 DMW-J_022509 DMW-K_022509 Acetone 1,4-Dioxane 660-27893-37 8260B IMW-F_022509 cis-1,2-Dichloroethene Trichloroethene Vinyl chloride Carbon disulfide 1,4-Dioxane 660-27893-36 ug/L IDPT-14_022509 Carbon disulfide 1,4-Dioxane 660-27893-35 1.0 0.77 Acetone Carbon disulfide 1,4-Dioxane 660-27893-34 Method IDPT-13_022509 cis-1,2-Dichloroethene Trichloroethene 1,4-Dioxane 660-27893-33 Units 5.5 1,4-Dioxane 660-27893-32 Reporting Limit IDPT-10_022509 Toluene 660-27893-31 Job Number: 660-27893-1 DMW-L_022509 TestAmerica Tampa Page 5 of 221 04/06/2009 EXECUTIVE SUMMARY - Detections Client: ARCADIS U.S., Inc. Lab Sample ID Analyte 660-27893-38 Client Sample ID Result / Qualifier Units Method 1.0 ug/L 8260C SIM/ID 8800 59 1000 50 ug/L ug/L 8260B 8260C SIM/ID 310 290 12 0.54 170 36 150 150 580 65 23 8.7 3.3 1.2 2.1 0.050 1.0 0.50 1.0 1.0 10 5.0 20 2.0 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L SM 2340B SM 2340B SM 2340B 300.0 300.0 300.0 SM 2320B SM 2320B SM 2540C SM 2540D SM 5220D SM 5310C 0.20 0.0040 mg/L mg/L 6010B 6010B 0.50 0.20 1.0 0.080 0.0040 0.50 mg/L mg/L mg/L mg/L mg/L mg/L 6010B 6010B 6010B 6010B 6010B 6010B 0.97 I DUPE H_022509 Acetone 1,4-Dioxane 660-27893-41 Reporting Limit DUPE D_022509 1,4-Dioxane 660-27893-39 Job Number: 660-27893-1 IDPT-14_022509 Hardness as calcium carbonate Calcium hardness as calcium carbonate Magnesium hardness as calcium carbonate Bromide Chloride Sulfate Alkalinity Bicarbonate Alkalinity as CaCO3 Total Dissolved Solids Total Suspended Solids Chemical Oxygen Demand Total Organic Carbon J3 J3 Dissolved Iron, Dissolved Manganese, Dissolved 9.0 0.0065 Total Recoverable Calcium Iron Potassium Magnesium Manganese Sodium 120 9.7 1.2 2.8 0.0072 45 J3 J3 TestAmerica Tampa Page 6 of 221 04/06/2009 EXECUTIVE SUMMARY - Detections Client: ARCADIS U.S., Inc. Lab Sample ID Analyte 660-27893-42 Job Number: 660-27893-1 Client Sample ID Reporting Limit Units Method 3.3 1.2 2.1 0.050 0.50 0.50 1.0 1.0 10 1.0 20 1.0 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L SM 2340B SM 2340B SM 2340B 300.0 300.0 300.0 SM 2320B SM 2320B SM 2540C SM 2540D SM 5220D SM 5310C 2.6 0.0066 0.20 0.0040 mg/L mg/L 6010B 6010B 99 2.6 0.45 2.5 0.0065 17 0.50 0.20 1.0 0.080 0.0040 0.50 mg/L mg/L mg/L mg/L mg/L mg/L 6010B 6010B 6010B 6010B 6010B 6010B Result / Qualifier DMW-F_022509 Hardness as calcium carbonate Calcium hardness as calcium carbonate Magnesium hardness as calcium carbonate Bromide Chloride Sulfate Alkalinity Bicarbonate Alkalinity as CaCO3 Total Dissolved Solids Total Suspended Solids Chemical Oxygen Demand Total Organic Carbon 260 250 10 0.13 40 19 230 230 360 12 14 5.8 I Dissolved Iron, Dissolved Manganese, Dissolved Total Recoverable Calcium Iron Potassium Magnesium Manganese Sodium I TestAmerica Tampa Page 7 of 221 04/06/2009 EXECUTIVE SUMMARY - Detections Client: ARCADIS U.S., Inc. Lab Sample ID Analyte 660-27893-43 Job Number: 660-27893-1 Client Sample ID Reporting Limit Units Method 3.3 1.2 2.1 0.050 2.0 0.50 1.0 1.0 10 1.1 20 1.0 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L SM 2340B SM 2340B SM 2340B 300.0 300.0 300.0 SM 2320B SM 2320B SM 2540C SM 2540D SM 5220D SM 5310C 12 0.0083 0.20 0.0040 mg/L mg/L 6010B 6010B 160 13 0.70 3.6 0.0084 64 0.50 0.20 1.0 0.080 0.0040 0.50 mg/L mg/L mg/L mg/L mg/L mg/L 6010B 6010B 6010B 6010B 6010B 6010B Result / Qualifier DMW-J_022509 Hardness as calcium carbonate Calcium hardness as calcium carbonate Magnesium hardness as calcium carbonate Bromide Chloride Sulfate Alkalinity Bicarbonate Alkalinity as CaCO3 Total Dissolved Solids Total Suspended Solids Chemical Oxygen Demand Total Organic Carbon 420 400 15 0.47 270 54 180 180 780 27 14 5.5 I Dissolved Iron, Dissolved Manganese, Dissolved Total Recoverable Calcium Iron Potassium Magnesium Manganese Sodium I TestAmerica Tampa Page 8 of 221 04/06/2009 EXECUTIVE SUMMARY - Detections Client: ARCADIS U.S., Inc. Lab Sample ID Analyte 660-27893-44 Job Number: 660-27893-1 Client Sample ID Reporting Limit Units Method 200 190 7.9 35 8.6 200 200 270 26 3.0 3.3 1.2 2.1 0.50 0.50 1.0 1.0 5.0 1.7 1.0 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L SM 2340B SM 2340B SM 2340B 300.0 300.0 SM 2320B SM 2320B SM 2540C SM 2540D SM 5310C 4.0 0.0051 0.20 0.0040 mg/L mg/L 6010B 6010B 78 4.2 0.35 1.9 0.0052 17 0.50 0.20 1.0 0.080 0.0040 0.50 mg/L mg/L mg/L mg/L mg/L mg/L 6010B 6010B 6010B 6010B 6010B 6010B Result / Qualifier DMW-L_022509 Hardness as calcium carbonate Calcium hardness as calcium carbonate Magnesium hardness as calcium carbonate Chloride Sulfate Alkalinity Bicarbonate Alkalinity as CaCO3 Total Dissolved Solids Total Suspended Solids Total Organic Carbon Dissolved Iron, Dissolved Manganese, Dissolved Total Recoverable Calcium Iron Potassium Magnesium Manganese Sodium I TestAmerica Tampa Page 9 of 221 04/06/2009 EXECUTIVE SUMMARY - Detections Client: ARCADIS U.S., Inc. Lab Sample ID Analyte 660-27893-45 Job Number: 660-27893-1 Client Sample ID Reporting Limit Units Method 240 230 11 0.22 75 2.0 180 180 340 32 26 8.7 3.3 1.2 2.1 0.050 0.50 0.50 1.0 1.0 10 1.7 20 1.0 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L SM 2340B SM 2340B SM 2340B 300.0 300.0 300.0 SM 2320B SM 2320B SM 2540C SM 2540D SM 5220D SM 5310C 2.2 0.0068 0.20 0.0040 mg/L mg/L 6010B 6010B 93 2.5 0.50 2.8 0.0051 14 0.50 0.20 1.0 0.080 0.0040 0.50 mg/L mg/L mg/L mg/L mg/L mg/L 6010B 6010B 6010B 6010B 6010B 6010B Result / Qualifier DMW-I_022509 Hardness as calcium carbonate Calcium hardness as calcium carbonate Magnesium hardness as calcium carbonate Bromide Chloride Sulfate Alkalinity Bicarbonate Alkalinity as CaCO3 Total Dissolved Solids Total Suspended Solids Chemical Oxygen Demand Total Organic Carbon Dissolved Iron, Dissolved Manganese, Dissolved Total Recoverable Calcium Iron Potassium Magnesium Manganese Sodium I TestAmerica Tampa Page 10 of 221 04/06/2009 EXECUTIVE SUMMARY - Detections Client: ARCADIS U.S., Inc. Lab Sample ID Analyte 660-27893-46 Job Number: 660-27893-1 Client Sample ID Reporting Limit Units Method 260 250 8.7 41 71 130 130 320 3.9 6.8 3.3 1.2 2.1 0.50 0.50 1.0 1.0 10 1.0 1.0 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L SM 2340B SM 2340B SM 2340B 300.0 300.0 SM 2320B SM 2320B SM 2540C SM 2540D SM 5310C 3.4 0.023 0.20 0.0040 mg/L mg/L 6010B 6010B 100 3.5 0.54 2.1 0.025 13 0.50 0.20 1.0 0.080 0.0040 0.50 mg/L mg/L mg/L mg/L mg/L mg/L 6010B 6010B 6010B 6010B 6010B 6010B Result / Qualifier DMW-C_022609 Hardness as calcium carbonate Calcium hardness as calcium carbonate Magnesium hardness as calcium carbonate Chloride Sulfate Alkalinity Bicarbonate Alkalinity as CaCO3 Total Dissolved Solids Total Suspended Solids Total Organic Carbon Dissolved Iron, Dissolved Manganese, Dissolved Total Recoverable Calcium Iron Potassium Magnesium Manganese Sodium I TestAmerica Tampa Page 11 of 221 04/06/2009 EXECUTIVE SUMMARY - Detections Client: ARCADIS U.S., Inc. Lab Sample ID Analyte 660-27893-47 Job Number: 660-27893-1 Client Sample ID Reporting Limit Units Method 140 110 23 0.29 83 8.5 1.4 61 61 380 500 45 5.8 3.3 1.2 2.1 0.050 0.50 0.50 0.50 1.0 1.0 5.0 20 20 4.0 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L SM 2340B SM 2340B SM 2340B 300.0 300.0 300.0 353.2 SM 2320B SM 2320B SM 2540C SM 2540D SM 5220D SM 5310C 3.3 0.0060 0.20 0.0040 mg/L mg/L 6010B 6010B 46 7.2 1.4 5.6 0.0089 19 0.50 0.20 1.0 0.080 0.0040 0.50 mg/L mg/L mg/L mg/L mg/L mg/L 6010B 6010B 6010B 6010B 6010B 6010B Result / Qualifier IDPT-9_022609 Hardness as calcium carbonate Calcium hardness as calcium carbonate Magnesium hardness as calcium carbonate Bromide Chloride Sulfate Nitrite as N Alkalinity Bicarbonate Alkalinity as CaCO3 Total Dissolved Solids Total Suspended Solids Chemical Oxygen Demand Total Organic Carbon Dissolved Iron, Dissolved Manganese, Dissolved Total Recoverable Calcium Iron Potassium Magnesium Manganese Sodium TestAmerica Tampa Page 12 of 221 04/06/2009 EXECUTIVE SUMMARY - Detections Client: ARCADIS U.S., Inc. Lab Sample ID Analyte 660-27893-48 Job Number: 660-27893-1 Client Sample ID Reporting Limit Units Method 3.3 1.2 2.1 0.050 2.0 0.50 1.0 1.0 10 1.7 20 1.0 mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L SM 2340B SM 2340B SM 2340B 300.0 300.0 300.0 SM 2320B SM 2320B SM 2540C SM 2540D SM 5220D SM 5310C 11 0.012 0.20 0.0040 mg/L mg/L 6010B 6010B 61 9.6 1.0 2.5 0.011 27 0.50 0.20 1.0 0.080 0.0040 0.50 mg/L mg/L mg/L mg/L mg/L mg/L 6010B 6010B 6010B 6010B 6010B 6010B Result / Qualifier IDPT-15_022609 Hardness as calcium carbonate Calcium hardness as calcium carbonate Magnesium hardness as calcium carbonate Bromide Chloride Sulfate Alkalinity Bicarbonate Alkalinity as CaCO3 Total Dissolved Solids Total Suspended Solids Chemical Oxygen Demand Total Organic Carbon 160 150 10 0.52 170 6.1 37 37 410 22 11 5.2 I Dissolved Iron, Dissolved Manganese, Dissolved Total Recoverable Calcium Iron Potassium Magnesium Manganese Sodium TestAmerica Tampa Page 13 of 221 04/06/2009 METHOD SUMMARY Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Description Lab Location Method Preparation Method Volatile Organic Compounds (GC/MS) Purge and Trap TAL TAM TAL TAM SW846 8260B SW846 5030B 1,4-Dioxane by SIM/Isotopic Dilution Purge and Trap TAL TAM TAL TAM SW846 8260C SIM/ID SW846 5030B Metals (ICP) Sample Filtration, Field Preparation, Total Recoverable or Dissolved Metals TAL TAM TAL TAM TAL TAM SW846 6010B Hardness, Calculation TAL TAM SM SM 2340B Anions, Ion Chromatography TAL TAM MCAWW 300.0 Nitrogen, Nitrate-Nitrite Nitrogen, Nitrate-Nitrite TAL TAM TAL TAM MCAWW 353.2 Alkalinity TAL TAM SM SM 2320B Solids, Total Dissolved (TDS) TAL TAL SM SM 2540C Solids, Total Suspended (TSS) TAL TAL SM SM 2540D COD TAL TAM TAL TAM SM SM 5220D TAL TAM SM SM 5310C Matrix Water COD TOC FIELD_FLTRD SW846 3005A MCAWW 353.2 SM SM 5220 Lab References: TAL TAL = TestAmerica Tallahassee TAL TAM = TestAmerica Tampa Method References: MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions. SM = "Standard Methods For The Examination Of Water And Wastewater", SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. TestAmerica Tampa Page 14 of 221 04/06/2009 METHOD / ANALYST SUMMARY Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Method Analyst Analyst ID SW846 8260B SW846 8260B Carlson, Robyn Mathew, Pinky RC PM SW846 8260C SIM/ID SW846 8260C SIM/ID Carlson, Robyn Mathew, Pinky RC PM SW846 6010B Fox, Greg GF SM SM 2340B Fox, Greg GF MCAWW 300.0 Alvarez, Luz LA MCAWW 353.2 Steward, Tiffany TS SM SM 2320B Steward, Tiffany TS SM SM 2540C Frank, Michelle MF SM SM 2540D Frank, Michelle MF SM SM 5220D Martin, Randolph RM SM SM 5310C Martin, Randolph RM TestAmerica Tampa Page 15 of 221 04/06/2009 SAMPLE SUMMARY Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Lab Sample ID Client Sample ID Client Matrix 660-27893-1 660-27893-2 660-27893-3 660-27893-4 660-27893-5 660-27893-6 660-27893-7 660-27893-8 660-27893-9 660-27893-10 660-27893-11 660-27893-12 660-27893-13 660-27893-14 660-27893-15 660-27893-16 660-27893-17 660-27893-18 660-27893-19 660-27893-20 660-27893-21 660-27893-22 660-27893-23 660-27893-24 660-27893-25 660-27893-26 660-27893-27 660-27893-28 660-27893-29 660-27893-30 660-27893-31 660-27893-32 660-27893-33 660-27893-34 660-27893-35 660-27893-36 660-27893-37 660-27893-38 660-27893-39 660-27893-40 660-27893-41 660-27893-42 660-27893-43 660-27893-44 660-27893-45 660-27893-46 DMW-P_022509 DMW-O_022509 DMW-Q_022509 DMW-C_022509 IMW-D_022509 DMW-B_022509 IDPT-15_022509 DMW-8_022509 SMW-D_022509 IDPT-8_022509 IDPT-9_022509 SMW-E_022509 SMW-H_022509 DMW-N_022509 DUPE E_022509 SMW-I_022509 DMW-I_022509 SMW-N_022509 IDPT-12_022509 IMW-J_022509 DMW-A_022509 DMW-W_022509 H-1_022509 SMW-A_022509 Trip Blank 3_022509 IDPT-1_022509 IDPT-2_022509 IDPT-5_022509 IDPT-6_022509 IDPT-10_022509 IDPT-13_022509 IDPT-14_022509 IMW-F_022509 DMW-F_022509 DMW-J_022509 DMW-K_022509 DMW-L_022509 DUPE D_022509 DUPE H_022509 Trip Blank_022509 IDPT-14_022509 DMW-F_022509 DMW-J_022509 DMW-L_022509 DMW-I_022509 DMW-C_022609 Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Date/Time Sampled 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/25/2009 02/26/2009 0857 0944 1013 1112 1154 1238 1425 1553 1614 1648 1730 1814 1405 1055 0000 1130 1440 1020 1640 1540 1200 0946 1300 1235 0000 1555 1654 1422 1725 1626 1455 1317 0918 0828 1216 0954 1105 0000 0000 0000 1317 0828 1216 1105 1440 0755 Date/Time Received 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 02/26/2009 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 TestAmerica Tampa Page 16 of 221 04/06/2009 SAMPLE SUMMARY Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Lab Sample ID Client Sample ID Client Matrix 660-27893-47 660-27893-48 IDPT-9_022609 IDPT-15_022609 Water Water Date/Time Sampled Date/Time Received 02/26/2009 0745 02/26/2009 0805 02/26/2009 1030 02/26/2009 1030 TestAmerica Tampa Page 17 of 221 04/06/2009 SAMPLE RESULTS TestAmerica Tampa Page 18 of 221 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-P_022509 Lab Sample ID: Client Matrix: 660-27893-1 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 0857 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/27/2009 1634 02/27/2009 1634 Analysis Batch: 660-75524 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 2.8 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 19 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HB2729.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-P_022509 Lab Sample ID: Client Matrix: 660-27893-1 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 0857 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/27/2009 1634 02/27/2009 1634 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75524 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 101 78 98 Page 20 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HB2729.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-O_022509 Lab Sample ID: Client Matrix: 660-27893-2 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 0944 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/27/2009 1651 02/27/2009 1651 Analysis Batch: 660-75524 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 21 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HB2730.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-O_022509 Lab Sample ID: Client Matrix: 660-27893-2 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 0944 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/27/2009 1651 02/27/2009 1651 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75524 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 98 77 101 Page 22 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HB2730.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-Q_022509 Lab Sample ID: Client Matrix: 660-27893-3 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1013 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/27/2009 1708 02/27/2009 1708 Analysis Batch: 660-75524 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 23 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HB2731.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-Q_022509 Lab Sample ID: Client Matrix: 660-27893-3 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1013 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/27/2009 1708 02/27/2009 1708 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75524 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 45 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 116 82 100 Page 24 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HB2731.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-C_022509 Lab Sample ID: Client Matrix: 660-27893-4 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1112 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/27/2009 1725 02/27/2009 1725 Analysis Batch: 660-75524 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 25 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HB2732.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-C_022509 Lab Sample ID: Client Matrix: 660-27893-4 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1112 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/27/2009 1725 02/27/2009 1725 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75524 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 105 89 106 Page 26 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HB2732.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IMW-D_022509 Lab Sample ID: Client Matrix: 660-27893-5 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1154 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/27/2009 1743 02/27/2009 1743 Analysis Batch: 660-75524 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 27 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HB2733.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IMW-D_022509 Lab Sample ID: Client Matrix: 660-27893-5 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1154 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/27/2009 1743 02/27/2009 1743 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75524 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 101 84 95 Page 28 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HB2733.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-B_022509 Lab Sample ID: Client Matrix: 660-27893-6 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1238 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/27/2009 1800 02/27/2009 1800 Analysis Batch: 660-75524 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 29 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HB2734.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-B_022509 Lab Sample ID: Client Matrix: 660-27893-6 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1238 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/27/2009 1800 02/27/2009 1800 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75524 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 105 81 101 Page 30 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HB2734.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IDPT-15_022509 Lab Sample ID: Client Matrix: 660-27893-7 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1425 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/27/2009 1817 02/27/2009 1817 Analysis Batch: 660-75524 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 4.3 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 31 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HB2735.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IDPT-15_022509 Lab Sample ID: Client Matrix: 660-27893-7 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1425 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/27/2009 1817 02/27/2009 1817 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75524 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 107 86 103 Page 32 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HB2735.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-8_022509 Lab Sample ID: Client Matrix: 660-27893-8 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1553 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/27/2009 1834 02/27/2009 1834 Analysis Batch: 660-75524 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 33 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HB2736.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-8_022509 Lab Sample ID: Client Matrix: 660-27893-8 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1553 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/27/2009 1834 02/27/2009 1834 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75524 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 104 88 101 Page 34 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HB2736.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: SMW-D_022509 Lab Sample ID: Client Matrix: 660-27893-9 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1614 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1229 03/02/2009 1229 Analysis Batch: 660-75614 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 35 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0215.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: SMW-D_022509 Lab Sample ID: Client Matrix: 660-27893-9 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1614 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1229 03/02/2009 1229 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75614 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 101 79 105 Page 36 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0215.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IDPT-8_022509 Lab Sample ID: Client Matrix: 660-27893-10 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1648 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1212 03/02/2009 1212 Analysis Batch: 660-75614 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 1.9 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 37 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0214.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IDPT-8_022509 Lab Sample ID: Client Matrix: 660-27893-10 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1648 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1212 03/02/2009 1212 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75614 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 92 82 107 Page 38 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0214.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IDPT-9_022509 Lab Sample ID: Client Matrix: 660-27893-11 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1730 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1247 03/02/2009 1247 Analysis Batch: 660-75614 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 39 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0216.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IDPT-9_022509 Lab Sample ID: Client Matrix: 660-27893-11 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1730 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1247 03/02/2009 1247 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75614 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 101 86 108 Page 40 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0216.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: SMW-E_022509 Lab Sample ID: Client Matrix: 660-27893-12 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1814 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1304 03/02/2009 1304 Analysis Batch: 660-75614 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 41 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0217.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: SMW-E_022509 Lab Sample ID: Client Matrix: 660-27893-12 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1814 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1304 03/02/2009 1304 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75614 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 99 87 108 Page 42 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0217.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: SMW-H_022509 Lab Sample ID: Client Matrix: 660-27893-13 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1405 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1739 03/02/2009 1739 Analysis Batch: 660-75614 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 43 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0233.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: SMW-H_022509 Lab Sample ID: Client Matrix: 660-27893-13 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1405 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1739 03/02/2009 1739 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75614 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 95 86 107 Page 44 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0233.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-N_022509 Lab Sample ID: Client Matrix: 660-27893-14 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1055 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1321 03/02/2009 1321 Analysis Batch: 660-75614 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.1 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 45 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0218.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U I U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-N_022509 Lab Sample ID: Client Matrix: 660-27893-14 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1055 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1321 03/02/2009 1321 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75614 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 94 84 110 Page 46 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0218.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DUPE E_022509 Lab Sample ID: Client Matrix: 660-27893-15 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 0000 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1447 03/02/2009 1447 Analysis Batch: 660-75614 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 47 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0223.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DUPE E_022509 Lab Sample ID: Client Matrix: 660-27893-15 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 0000 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1447 03/02/2009 1447 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75614 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 103 90 106 Page 48 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0223.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: SMW-I_022509 Lab Sample ID: Client Matrix: 660-27893-16 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1130 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1430 03/02/2009 1430 Analysis Batch: 660-75614 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 49 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0222.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: SMW-I_022509 Lab Sample ID: Client Matrix: 660-27893-16 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1130 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1430 03/02/2009 1430 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75614 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 103 87 106 Page 50 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0222.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-I_022509 Lab Sample ID: Client Matrix: 660-27893-17 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1440 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1338 03/02/2009 1338 Analysis Batch: 660-75614 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 51 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0219.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-I_022509 Lab Sample ID: Client Matrix: 660-27893-17 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1440 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1338 03/02/2009 1338 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75614 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 118 84 107 Page 52 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0219.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-I_022509 Lab Sample ID: Client Matrix: 660-27893-17 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1440 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 2.0 03/03/2009 1303 03/03/2009 1303 Analysis Batch: 660-75683 Run Type: DL Analyte Acetone Result (ug/L) 920 TestAmerica Tampa Page 53 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0316.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier MDL 20 PQL 40 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: SMW-N_022509 Lab Sample ID: Client Matrix: 660-27893-18 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1020 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1412 03/02/2009 1412 Analysis Batch: 660-75614 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 54 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0221.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: SMW-N_022509 Lab Sample ID: Client Matrix: 660-27893-18 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1020 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1412 03/02/2009 1412 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75614 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 103 84 108 Page 55 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0221.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IDPT-12_022509 Lab Sample ID: Client Matrix: 660-27893-19 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1640 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1355 03/02/2009 1355 Analysis Batch: 660-75614 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 56 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0220.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IDPT-12_022509 Lab Sample ID: Client Matrix: 660-27893-19 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1640 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1355 03/02/2009 1355 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75614 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 98 90 109 Page 57 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0220.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IMW-J_022509 Lab Sample ID: Client Matrix: 660-27893-20 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1540 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1521 03/02/2009 1521 Analysis Batch: 660-75614 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 58 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0225.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IMW-J_022509 Lab Sample ID: Client Matrix: 660-27893-20 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1540 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1521 03/02/2009 1521 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75614 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 101 91 110 Page 59 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0225.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IMW-J_022509 Lab Sample ID: Client Matrix: 660-27893-20 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1540 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 2.0 03/03/2009 1321 03/03/2009 1321 Analysis Batch: 660-75683 Run Type: DL Analyte Acetone Result (ug/L) 1300 TestAmerica Tampa Page 60 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0317.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier MDL 20 PQL 40 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-A_022509 Lab Sample ID: Client Matrix: 660-27893-21 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1200 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/28/2009 0140 02/28/2009 0140 Analysis Batch: 660-75698 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 61 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JB2729.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-A_022509 Lab Sample ID: Client Matrix: 660-27893-21 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1200 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/28/2009 0140 02/28/2009 0140 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75698 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 99 100 99 Page 62 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JB2729.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-W_022509 Lab Sample ID: Client Matrix: 660-27893-22 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 0946 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1538 03/02/2009 1538 Analysis Batch: 660-75700 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 63 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0214.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-W_022509 Lab Sample ID: Client Matrix: 660-27893-22 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 0946 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1538 03/02/2009 1538 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75700 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 102 105 98 Page 64 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0214.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: H-1_022509 Lab Sample ID: Client Matrix: 660-27893-23 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1300 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1651 03/02/2009 1651 Analysis Batch: 660-75700 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.83 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 65 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0217.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier I U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: H-1_022509 Lab Sample ID: Client Matrix: 660-27893-23 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1300 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1651 03/02/2009 1651 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75700 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 101 100 98 Page 66 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0217.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: SMW-A_022509 Lab Sample ID: Client Matrix: 660-27893-24 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1235 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1715 03/02/2009 1715 Analysis Batch: 660-75700 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 67 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0218.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: SMW-A_022509 Lab Sample ID: Client Matrix: 660-27893-24 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1235 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1715 03/02/2009 1715 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75700 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 102 105 101 Page 68 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0218.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: Trip Blank 3_022509 Lab Sample ID: Client Matrix: 660-27893-25 Water Date Sampled: Date Received: 02/25/2009 0000 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/28/2009 0955 02/28/2009 0955 Analysis Batch: 660-75699 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 69 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JB2749.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: Trip Blank 3_022509 Lab Sample ID: Client Matrix: 660-27893-25 Water Date Sampled: Date Received: 02/25/2009 0000 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/28/2009 0955 02/28/2009 0955 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75699 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 101 101 97 Page 70 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JB2749.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IDPT-1_022509 Lab Sample ID: Client Matrix: 660-27893-26 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1555 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/28/2009 1019 02/28/2009 1019 Analysis Batch: 660-75699 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 1.1 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 71 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JB2750.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IDPT-1_022509 Lab Sample ID: Client Matrix: 660-27893-26 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1555 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/28/2009 1019 02/28/2009 1019 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75699 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.51 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 100 101 100 Page 72 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JB2750.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U I U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IDPT-2_022509 Lab Sample ID: Client Matrix: 660-27893-27 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1654 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/28/2009 1132 02/28/2009 1132 Analysis Batch: 660-75699 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 73 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JB2753.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IDPT-2_022509 Lab Sample ID: Client Matrix: 660-27893-27 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1654 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/28/2009 1132 02/28/2009 1132 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75699 Result (ug/L) 0.15 0.50 13 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 1.8 %Rec 100 102 102 Page 74 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JB2753.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U I MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IDPT-5_022509 Lab Sample ID: Client Matrix: 660-27893-28 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1422 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/28/2009 1156 02/28/2009 1156 Analysis Batch: 660-75699 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 75 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JB2754.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IDPT-5_022509 Lab Sample ID: Client Matrix: 660-27893-28 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1422 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/28/2009 1156 02/28/2009 1156 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75699 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 100 99 100 Page 76 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JB2754.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IDPT-6_022509 Lab Sample ID: Client Matrix: 660-27893-29 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1725 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/28/2009 1221 02/28/2009 1221 Analysis Batch: 660-75699 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 16 0.57 0.59 4.0 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 77 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JB2755.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U I U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IDPT-6_022509 Lab Sample ID: Client Matrix: 660-27893-29 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1725 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/28/2009 1221 02/28/2009 1221 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75699 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 101 102 104 Page 78 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JB2755.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IDPT-6_022509 Lab Sample ID: Client Matrix: 660-27893-29 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1725 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 5.0 03/02/2009 2005 03/02/2009 2005 Analysis Batch: 660-75700 Run Type: DL Analyte Vinyl chloride Result (ug/L) 330 TestAmerica Tampa Page 79 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0225.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier MDL 2.5 PQL 5.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IDPT-10_022509 Lab Sample ID: Client Matrix: 660-27893-30 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1626 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1804 03/02/2009 1804 Analysis Batch: 660-75700 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 80 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0220.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IDPT-10_022509 Lab Sample ID: Client Matrix: 660-27893-30 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1626 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1804 03/02/2009 1804 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75700 Result (ug/L) 0.15 0.50 5.5 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 103 104 102 Page 81 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0220.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IDPT-13_022509 Lab Sample ID: Client Matrix: 660-27893-31 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1455 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/28/2009 1310 02/28/2009 1310 Analysis Batch: 660-75699 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 82 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JB2757.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IDPT-13_022509 Lab Sample ID: Client Matrix: 660-27893-31 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1455 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/28/2009 1310 02/28/2009 1310 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75699 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 101 103 101 Page 83 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JB2757.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IDPT-14_022509 Lab Sample ID: Client Matrix: 660-27893-32 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1317 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 50 03/02/2009 2030 03/02/2009 2030 Analysis Batch: 660-75700 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 25 29 29 18 29 120 34 32 42 21 32 120 45 50 32 26 17 120 25 20 22 32 26 120 26 28 22 470 22 26 20 18 16 7.0 7.0 22 20 9.5 34 200 120 30 49 32 TestAmerica Tampa Page 84 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0226.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 25 29 29 18 29 120 34 32 42 21 32 120 45 50 32 26 17 120 25 20 22 32 26 120 26 28 22 32 22 26 20 18 16 7.0 7.0 22 20 9.5 34 200 120 30 49 32 PQL 50 50 50 50 50 250 50 50 50 50 50 250 50 200 50 50 50 250 50 50 50 50 50 250 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 250 250 50 100 50 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IDPT-14_022509 Lab Sample ID: Client Matrix: 660-27893-32 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1317 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 50 03/02/2009 2030 03/02/2009 2030 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75700 Result (ug/L) 7.5 25 26 38 29 23 24 3800 120 9.0 43 27 25 25 500 420 190 42 220 22 30 %Rec 101 102 101 Page 85 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0226.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U MDL 7.5 25 26 38 29 23 24 25 120 9.0 43 27 25 25 500 420 190 42 220 22 30 PQL 50 50 50 50 50 50 50 50 250 50 50 50 50 50 1000 500 500 50 500 50 100 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IMW-F_022509 Lab Sample ID: Client Matrix: 660-27893-33 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 0918 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1852 03/02/2009 1852 Analysis Batch: 660-75700 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 86 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0222.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IMW-F_022509 Lab Sample ID: Client Matrix: 660-27893-33 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 0918 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1852 03/02/2009 1852 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75700 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 160 8.4 3.8 1.0 4.4 0.44 0.60 %Rec 101 104 102 Page 87 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0222.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-F_022509 Lab Sample ID: Client Matrix: 660-27893-34 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 0828 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 2.0 03/02/2009 2054 03/02/2009 2054 Analysis Batch: 660-75700 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 1.0 1.2 1.2 0.70 1.2 5.0 1.3 1.3 1.7 0.84 1.3 5.0 1.8 2.0 1.3 1.0 0.68 5.0 1.0 0.82 0.88 1.3 1.0 5.0 1.0 1.1 0.90 1.3 0.88 1.0 0.78 0.72 0.62 0.28 0.28 0.88 0.80 0.38 1.4 8.0 5.0 1.2 2.0 1.3 TestAmerica Tampa Page 88 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0227.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 1.0 1.2 1.2 0.70 1.2 5.0 1.3 1.3 1.7 0.84 1.3 5.0 1.8 2.0 1.3 1.0 0.68 5.0 1.0 0.82 0.88 1.3 1.0 5.0 1.0 1.1 0.90 1.3 0.88 1.0 0.78 0.72 0.62 0.28 0.28 0.88 0.80 0.38 1.4 8.0 5.0 1.2 2.0 1.3 PQL 2.0 2.0 2.0 2.0 2.0 10 2.0 2.0 2.0 2.0 2.0 10 2.0 8.0 2.0 2.0 2.0 10 2.0 2.0 2.0 2.0 2.0 10 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 10 10 2.0 4.0 2.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-F_022509 Lab Sample ID: Client Matrix: 660-27893-34 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 0828 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 2.0 03/02/2009 2054 03/02/2009 2054 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75700 Result (ug/L) 0.30 1.0 1.0 1.5 1.2 0.92 0.94 1.0 5.0 0.36 1.7 1.1 1.0 1.0 20 17 7.6 3.4 8.8 0.88 1.2 %Rec 103 101 104 Page 89 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0227.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U MDL 0.30 1.0 1.0 1.5 1.2 0.92 0.94 1.0 5.0 0.36 1.7 1.1 1.0 1.0 20 17 7.6 1.7 8.8 0.88 1.2 PQL 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 10 2.0 2.0 2.0 2.0 2.0 40 20 20 2.0 20 2.0 4.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-J_022509 Lab Sample ID: Client Matrix: 660-27893-35 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1216 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/28/2009 1447 02/28/2009 1447 Analysis Batch: 660-75699 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 36 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 90 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JB2761.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-J_022509 Lab Sample ID: Client Matrix: 660-27893-35 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1216 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/28/2009 1447 02/28/2009 1447 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75699 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 14 2.5 0.18 0.86 0.54 2.7 0.50 9.9 8.4 3.8 1.5 4.4 0.44 0.60 %Rec 99 101 98 Page 91 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JB2761.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-K_022509 Lab Sample ID: Client Matrix: 660-27893-36 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 0954 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 20 03/02/2009 2119 03/02/2009 2119 Analysis Batch: 660-75700 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 10 12 12 7.0 12 50 13 13 17 8.4 13 50 18 20 13 10 6.8 50 10 8.2 8.8 13 10 50 10 11 9.0 13 8.8 10 7.8 7.2 6.2 2.8 2.8 8.8 8.0 3.8 14 80 50 12 20 13 TestAmerica Tampa Page 92 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0228.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 10 12 12 7.0 12 50 13 13 17 8.4 13 50 18 20 13 10 6.8 50 10 8.2 8.8 13 10 50 10 11 9.0 13 8.8 10 7.8 7.2 6.2 2.8 2.8 8.8 8.0 3.8 14 80 50 12 20 13 PQL 20 20 20 20 20 100 20 20 20 20 20 100 20 80 20 20 20 100 20 20 20 20 20 100 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 100 100 20 40 20 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-K_022509 Lab Sample ID: Client Matrix: 660-27893-36 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 0954 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 20 03/02/2009 2119 03/02/2009 2119 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75700 Result (ug/L) 3.0 10 10 15 12 9.2 9.4 10 50 3.6 17 11 10 10 9800 170 76 17 88 8.8 12 %Rec 101 102 98 Page 93 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0228.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U MDL 3.0 10 10 15 12 9.2 9.4 10 50 3.6 17 11 10 10 200 170 76 17 88 8.8 12 PQL 20 20 20 20 20 20 20 20 100 20 20 20 20 20 400 200 200 20 200 20 40 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-L_022509 Lab Sample ID: Client Matrix: 660-27893-37 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1105 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 2.0 03/02/2009 2144 03/02/2009 2144 Analysis Batch: 660-75700 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 1.0 1.2 1.2 0.70 1.2 5.0 1.3 1.3 1.7 0.84 1.3 5.0 1.8 2.0 1.3 1.0 0.68 5.0 1.0 0.82 0.88 1.3 1.0 5.0 1.0 1.1 0.90 1.3 0.88 1.0 0.78 0.72 0.62 0.28 0.28 0.88 0.80 0.38 1.4 8.0 5.0 1.2 2.0 1.3 TestAmerica Tampa Page 94 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0229.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 1.0 1.2 1.2 0.70 1.2 5.0 1.3 1.3 1.7 0.84 1.3 5.0 1.8 2.0 1.3 1.0 0.68 5.0 1.0 0.82 0.88 1.3 1.0 5.0 1.0 1.1 0.90 1.3 0.88 1.0 0.78 0.72 0.62 0.28 0.28 0.88 0.80 0.38 1.4 8.0 5.0 1.2 2.0 1.3 PQL 2.0 2.0 2.0 2.0 2.0 10 2.0 2.0 2.0 2.0 2.0 10 2.0 8.0 2.0 2.0 2.0 10 2.0 2.0 2.0 2.0 2.0 10 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 10 10 2.0 4.0 2.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-L_022509 Lab Sample ID: Client Matrix: 660-27893-37 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1105 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 2.0 03/02/2009 2144 03/02/2009 2144 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75700 Result (ug/L) 0.30 1.0 1.0 1.5 1.2 0.92 0.94 1.0 5.0 0.36 1.7 1.1 1.0 1.0 20 17 7.6 1.7 8.8 0.88 1.2 %Rec 103 104 100 Page 95 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0229.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.30 1.0 1.0 1.5 1.2 0.92 0.94 1.0 5.0 0.36 1.7 1.1 1.0 1.0 20 17 7.6 1.7 8.8 0.88 1.2 PQL 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 10 2.0 2.0 2.0 2.0 2.0 40 20 20 2.0 20 2.0 4.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DUPE D_022509 Lab Sample ID: Client Matrix: 660-27893-38 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 0000 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/28/2009 1600 02/28/2009 1600 Analysis Batch: 660-75699 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 TestAmerica Tampa Page 96 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JB2764.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DUPE D_022509 Lab Sample ID: Client Matrix: 660-27893-38 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 0000 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 02/28/2009 1600 02/28/2009 1600 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75699 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 100 101 100 Page 97 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JB2764.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DUPE H_022509 Lab Sample ID: Client Matrix: 660-27893-39 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 0000 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 50 03/02/2009 2208 03/02/2009 2208 Analysis Batch: 660-75700 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane Result (ug/L) 25 29 29 18 29 120 34 32 42 21 32 120 45 50 32 26 17 120 25 20 22 32 26 120 26 28 22 32 22 26 20 18 16 7.0 7.0 22 20 9.5 34 200 120 30 49 32 TestAmerica Tampa Page 98 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0230.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 25 29 29 18 29 120 34 32 42 21 32 120 45 50 32 26 17 120 25 20 22 32 26 120 26 28 22 32 22 26 20 18 16 7.0 7.0 22 20 9.5 34 200 120 30 49 32 PQL 50 50 50 50 50 250 50 50 50 50 50 250 50 200 50 50 50 250 50 50 50 50 50 250 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 250 250 50 100 50 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DUPE H_022509 Lab Sample ID: Client Matrix: 660-27893-39 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 0000 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 50 03/02/2009 2208 03/02/2009 2208 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75700 Result (ug/L) 7.5 25 26 38 29 23 24 25 120 9.0 43 27 25 25 8800 420 190 42 220 22 30 %Rec 102 102 101 Page 99 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0230.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U MDL 7.5 25 26 38 29 23 24 25 120 9.0 43 27 25 25 500 420 190 42 220 22 30 PQL 50 50 50 50 50 50 50 50 250 50 50 50 50 50 1000 500 500 50 500 50 100 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: Trip Blank_022509 Lab Sample ID: Client Matrix: 660-27893-40 Water Date Sampled: Date Received: 02/25/2009 0000 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1513 03/02/2009 1513 Analyte Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane TestAmerica Tampa Analysis Batch: 660-75700 Result (ug/L) 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 Page 100 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0213.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 PQL 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: Trip Blank_022509 Lab Sample ID: Client Matrix: 660-27893-40 Water Date Sampled: Date Received: 02/25/2009 0000 02/26/2009 1030 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 03/02/2009 1513 03/02/2009 1513 Analyte 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane TestAmerica Tampa Analysis Batch: 660-75700 Result (ug/L) 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 %Rec 102 106 98 Page 101 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0213.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U U U U U U U U U U U U U U U U U U U U U MDL 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 PQL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 77 - 122 74 - 126 70 - 130 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: DMW-P_022509 Lab Sample ID: Client Matrix: 660-27893-1 Water Date Sampled: Date Received: 02/25/2009 0857 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 02/27/2009 1634 02/27/2009 1634 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75525 Result (ug/L) 0.54 Page 102 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HB2729.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: DMW-O_022509 Lab Sample ID: Client Matrix: 660-27893-2 Water Date Sampled: Date Received: 02/25/2009 0944 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 02/27/2009 1651 02/27/2009 1651 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75525 Result (ug/L) 0.54 Page 103 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HB2730.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: DMW-Q_022509 Lab Sample ID: Client Matrix: 660-27893-3 Water Date Sampled: Date Received: 02/25/2009 1013 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 02/27/2009 1708 02/27/2009 1708 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75525 Result (ug/L) 0.54 Page 104 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HB2731.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: DMW-C_022509 Lab Sample ID: Client Matrix: 660-27893-4 Water Date Sampled: Date Received: 02/25/2009 1112 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 02/27/2009 1725 02/27/2009 1725 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75525 Result (ug/L) 16 Page 105 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HB2732.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: IMW-D_022509 Lab Sample ID: Client Matrix: 660-27893-5 Water Date Sampled: Date Received: 02/25/2009 1154 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 02/27/2009 1743 02/27/2009 1743 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75525 Result (ug/L) 5.2 Page 106 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HB2733.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: DMW-B_022509 Lab Sample ID: Client Matrix: 660-27893-6 Water Date Sampled: Date Received: 02/25/2009 1238 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 02/27/2009 1800 02/27/2009 1800 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75525 Result (ug/L) 0.54 Page 107 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HB2734.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: IDPT-15_022509 Lab Sample ID: Client Matrix: 660-27893-7 Water Date Sampled: Date Received: 02/25/2009 1425 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 02/27/2009 1817 02/27/2009 1817 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75525 Result (ug/L) 78 Page 108 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HB2735.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: DMW-8_022509 Lab Sample ID: Client Matrix: 660-27893-8 Water Date Sampled: Date Received: 02/25/2009 1553 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 03/02/2009 1538 03/02/2009 1538 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75613 Result (ug/L) 0.54 Page 109 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0226.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: SMW-D_022509 Lab Sample ID: Client Matrix: 660-27893-9 Water Date Sampled: Date Received: 02/25/2009 1614 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 03/02/2009 1229 03/02/2009 1229 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75613 Result (ug/L) 0.54 Page 110 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0215.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: IDPT-8_022509 Lab Sample ID: Client Matrix: 660-27893-10 Water Date Sampled: Date Received: 02/25/2009 1648 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 03/02/2009 1212 03/02/2009 1212 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75613 Result (ug/L) 20 Page 111 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0214.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: IDPT-9_022509 Lab Sample ID: Client Matrix: 660-27893-11 Water Date Sampled: Date Received: 02/25/2009 1730 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 03/02/2009 1247 03/02/2009 1247 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75613 Result (ug/L) 9.5 Page 112 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0216.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: SMW-E_022509 Lab Sample ID: Client Matrix: 660-27893-12 Water Date Sampled: Date Received: 02/25/2009 1814 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 03/02/2009 1304 03/02/2009 1304 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75613 Result (ug/L) 1.4 Page 113 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0217.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: SMW-H_022509 Lab Sample ID: Client Matrix: 660-27893-13 Water Date Sampled: Date Received: 02/25/2009 1405 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 03/03/2009 1246 03/03/2009 1246 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75684 Result (ug/L) 0.80 Page 114 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0315.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier I MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: DMW-N_022509 Lab Sample ID: Client Matrix: 660-27893-14 Water Date Sampled: Date Received: 02/25/2009 1055 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 03/02/2009 1321 03/02/2009 1321 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75613 Result (ug/L) 0.54 Page 115 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0218.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: DUPE E_022509 Lab Sample ID: Client Matrix: 660-27893-15 Water Date Sampled: Date Received: 02/25/2009 0000 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 03/02/2009 1447 03/02/2009 1447 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75613 Result (ug/L) 0.54 Page 116 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0223.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: SMW-I_022509 Lab Sample ID: Client Matrix: 660-27893-16 Water Date Sampled: Date Received: 02/25/2009 1130 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 03/02/2009 1430 03/02/2009 1430 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75613 Result (ug/L) 0.54 Page 117 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0222.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: DMW-I_022509 Lab Sample ID: Client Matrix: 660-27893-17 Water Date Sampled: Date Received: 02/25/2009 1440 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 03/02/2009 1338 03/02/2009 1338 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75613 Result (ug/L) 5.1 Page 118 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0219.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: SMW-N_022509 Lab Sample ID: Client Matrix: 660-27893-18 Water Date Sampled: Date Received: 02/25/2009 1020 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 03/02/2009 1412 03/02/2009 1412 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75613 Result (ug/L) 0.95 Page 119 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0221.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier I MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: IDPT-12_022509 Lab Sample ID: Client Matrix: 660-27893-19 Water Date Sampled: Date Received: 02/25/2009 1640 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 03/02/2009 1355 03/02/2009 1355 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75613 Result (ug/L) 27 Page 120 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0220.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: IMW-J_022509 Lab Sample ID: Client Matrix: 660-27893-20 Water Date Sampled: Date Received: 02/25/2009 1540 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 03/02/2009 1521 03/02/2009 1521 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75613 Result (ug/L) 0.54 Page 121 of 221 Instrument ID: BVMH GC/MS Lab File ID: 1HC0225.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: DMW-A_022509 Lab Sample ID: Client Matrix: 660-27893-21 Water Date Sampled: Date Received: 02/25/2009 1200 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 02/28/2009 0140 02/28/2009 0140 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75694 Result (ug/L) 0.54 Page 122 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JB2729.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: DMW-W_022509 Lab Sample ID: Client Matrix: 660-27893-22 Water Date Sampled: Date Received: 02/25/2009 0946 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 03/02/2009 1538 03/02/2009 1538 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75696 Result (ug/L) 0.54 Page 123 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0214.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: H-1_022509 Lab Sample ID: Client Matrix: 660-27893-23 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1300 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 03/02/2009 1651 03/02/2009 1651 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75696 Result (ug/L) 0.54 Page 124 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0217.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: SMW-A_022509 Lab Sample ID: Client Matrix: 660-27893-24 Water Date Sampled: Date Received: 02/25/2009 1235 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 03/02/2009 1715 03/02/2009 1715 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75696 Result (ug/L) 0.54 Page 125 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0218.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: Trip Blank 3_022509 Lab Sample ID: Client Matrix: 660-27893-25 Water Date Sampled: Date Received: 02/25/2009 0000 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 02/28/2009 0955 02/28/2009 0955 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75695 Result (ug/L) 0.54 Page 126 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JB2749.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: IDPT-1_022509 Lab Sample ID: Client Matrix: 660-27893-26 Water Date Sampled: Date Received: 02/25/2009 1555 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 02/28/2009 1019 02/28/2009 1019 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75695 Result (ug/L) 14 Page 127 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JB2750.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: IDPT-2_022509 Lab Sample ID: Client Matrix: 660-27893-27 Water Date Sampled: Date Received: 02/25/2009 1654 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 03/02/2009 1739 03/02/2009 1739 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75696 Result (ug/L) 0.54 Page 128 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0219.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: IDPT-5_022509 Lab Sample ID: Client Matrix: 660-27893-28 Water Date Sampled: Date Received: 02/25/2009 1422 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 02/28/2009 1156 02/28/2009 1156 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75695 Result (ug/L) 24 Page 129 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JB2754.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: IDPT-6_022509 Lab Sample ID: Client Matrix: 660-27893-29 Water Date Sampled: Date Received: 02/25/2009 1725 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 5.0 03/02/2009 2005 03/02/2009 2005 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75696 Result (ug/L) 100 Page 130 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0225.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier MDL 2.7 PQL 5.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: IDPT-10_022509 Lab Sample ID: Client Matrix: 660-27893-30 Water Date Sampled: Date Received: 02/25/2009 1626 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 03/02/2009 1804 03/02/2009 1804 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75696 Result (ug/L) 0.54 Page 131 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0220.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: IDPT-13_022509 Lab Sample ID: Client Matrix: 660-27893-31 Water Date Sampled: Date Received: 02/25/2009 1455 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 03/02/2009 1828 03/02/2009 1828 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75696 Result (ug/L) 0.77 Page 132 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0221.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier I MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: IDPT-14_022509 Lab Sample ID: Client Matrix: 660-27893-32 Water Date Sampled: Date Received: 02/25/2009 1317 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 50 03/02/2009 2030 03/02/2009 2030 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75696 Result (ug/L) 160 Page 133 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0226.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier MDL 27 PQL 50 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: IMW-F_022509 Lab Sample ID: Client Matrix: 660-27893-33 Water Date Sampled: Date Received: 02/25/2009 0918 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 03/02/2009 1852 03/02/2009 1852 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75696 Result (ug/L) 7.9 Page 134 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0222.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: DMW-F_022509 Lab Sample ID: Client Matrix: 660-27893-34 Water Date Sampled: Date Received: 02/25/2009 0828 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 2.0 03/02/2009 2054 03/02/2009 2054 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75696 Result (ug/L) 110 Page 135 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0227.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier MDL 1.1 PQL 2.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: DMW-J_022509 Lab Sample ID: Client Matrix: 660-27893-35 Water Date Sampled: Date Received: 02/25/2009 1216 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 03/02/2009 1917 03/02/2009 1917 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75696 Result (ug/L) 6.2 Page 136 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0223.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: DMW-K_022509 Lab Sample ID: Client Matrix: 660-27893-36 Water Date Sampled: Date Received: 02/25/2009 0954 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 20 03/02/2009 2119 03/02/2009 2119 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75696 Result (ug/L) 55 Page 137 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0228.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier MDL 11 PQL 20 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: DMW-L_022509 Lab Sample ID: Client Matrix: 660-27893-37 Water Date Sampled: Date Received: 02/25/2009 1105 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 2.0 03/02/2009 2144 03/02/2009 2144 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75696 Result (ug/L) 88 Page 138 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0229.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier MDL 1.1 PQL 2.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: DUPE D_022509 Lab Sample ID: Client Matrix: 660-27893-38 Water Date Sampled: Date Received: 02/25/2009 0000 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 03/02/2009 1941 03/02/2009 1941 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75696 Result (ug/L) 0.97 Page 139 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0224.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier I MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: DUPE H_022509 Lab Sample ID: Client Matrix: 660-27893-39 Water Date Sampled: Date Received: 02/25/2009 0000 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 50 03/02/2009 2208 03/02/2009 2208 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75696 Result (ug/L) 59 Page 140 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JC0230.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier MDL 27 PQL 50 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Client Sample ID: Trip Blank_022509 Lab Sample ID: Client Matrix: 660-27893-40 Water Date Sampled: Date Received: 02/25/2009 0000 02/26/2009 1030 8260C SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C SIM/ID 5030B 1.0 02/28/2009 1648 02/28/2009 1648 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-75695 Result (ug/L) 0.54 Page 141 of 221 Instrument ID: BVMJ GC/MS Lab File ID: 1JB2766.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Qualifier U MDL 0.54 PQL 1.0 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IDPT-14_022509 Lab Sample ID: Client Matrix: 660-27893-41 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1317 02/26/2009 1030 6010B Metals (ICP)-Total Recoverable Method: Preparation: Dilution: Date Analyzed: Date Prepared: 6010B 3005A 1.0 03/03/2009 1324 02/27/2009 1027 Analysis Batch: 660-75689 Prep Batch: 660-75517 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: TJA ICP TRACE 9C03A 50 mL 50 mL Analyte Result (mg/L) Qualifier MDL PQL Calcium Iron Potassium Magnesium Manganese Sodium 120 9.7 1.2 2.8 0.0072 45 J3 J3 0.10 0.050 0.19 0.020 0.0010 0.31 0.50 0.20 1.0 0.080 0.0040 0.50 6010B Metals (ICP)-Dissolved Method: Preparation: Dilution: Date Analyzed: Date Prepared: 6010B 3005A 1.0 03/03/2009 1351 02/27/2009 1027 Analysis Batch: 660-75689 Prep Batch: 660-75517 Analyte Result (mg/L) Iron, Dissolved Manganese, Dissolved 9.0 0.0065 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier TJA ICP TRACE 9C03A 50 mL 50 mL MDL PQL 0.050 0.0010 0.20 0.0040 SM 2340B Hardness, Calculation Method: Preparation: Dilution: Date Analyzed: Date Prepared: SM 2340B N/A 1.0 03/03/2009 1527 N/A Analysis Batch: 660-75708 Analyte Result (mg/L) Hardness as calcium carbonate Calcium hardness as calcium carbonate Magnesium hardness as calcium carbonate 310 290 12 TestAmerica Tampa Page 142 of 221 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier No Equipment N/A 1.0 mL PQL PQL 3.3 1.2 2.1 3.3 1.2 2.1 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-F_022509 Lab Sample ID: Client Matrix: 660-27893-42 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 0828 02/26/2009 1030 6010B Metals (ICP)-Total Recoverable Method: Preparation: Dilution: Date Analyzed: Date Prepared: 6010B 3005A 1.0 03/03/2009 1357 02/27/2009 1027 Analysis Batch: 660-75689 Prep Batch: 660-75517 Analyte Result (mg/L) Calcium Iron Potassium Magnesium Manganese Sodium 99 2.6 0.45 2.5 0.0065 17 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier I TJA ICP TRACE 9C03A 50 mL 50 mL MDL PQL 0.10 0.050 0.19 0.020 0.0010 0.31 0.50 0.20 1.0 0.080 0.0040 0.50 6010B Metals (ICP)-Dissolved Method: Preparation: Dilution: Date Analyzed: Date Prepared: 6010B 3005A 1.0 03/03/2009 1403 02/27/2009 1027 Analysis Batch: 660-75689 Prep Batch: 660-75517 Analyte Result (mg/L) Iron, Dissolved Manganese, Dissolved 2.6 0.0066 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier TJA ICP TRACE 9C03A 50 mL 50 mL MDL PQL 0.050 0.0010 0.20 0.0040 SM 2340B Hardness, Calculation Method: Preparation: Dilution: Date Analyzed: Date Prepared: SM 2340B N/A 1.0 03/03/2009 1527 N/A Analysis Batch: 660-75708 Analyte Result (mg/L) Hardness as calcium carbonate Calcium hardness as calcium carbonate Magnesium hardness as calcium carbonate 260 250 10 TestAmerica Tampa Page 143 of 221 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier No Equipment N/A 1.0 mL PQL PQL 3.3 1.2 2.1 3.3 1.2 2.1 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-J_022509 Lab Sample ID: Client Matrix: 660-27893-43 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1216 02/26/2009 1030 6010B Metals (ICP)-Total Recoverable Method: Preparation: Dilution: Date Analyzed: Date Prepared: 6010B 3005A 1.0 03/03/2009 1408 02/27/2009 1027 Analysis Batch: 660-75689 Prep Batch: 660-75517 Analyte Result (mg/L) Calcium Iron Potassium Magnesium Manganese Sodium 160 13 0.70 3.6 0.0084 64 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier I TJA ICP TRACE 9C03A 50 mL 50 mL MDL PQL 0.10 0.050 0.19 0.020 0.0010 0.31 0.50 0.20 1.0 0.080 0.0040 0.50 6010B Metals (ICP)-Dissolved Method: Preparation: Dilution: Date Analyzed: Date Prepared: 6010B 3005A 1.0 03/03/2009 1414 02/27/2009 1027 Analysis Batch: 660-75689 Prep Batch: 660-75517 Analyte Result (mg/L) Iron, Dissolved Manganese, Dissolved 12 0.0083 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier TJA ICP TRACE 9C03A 50 mL 50 mL MDL PQL 0.050 0.0010 0.20 0.0040 SM 2340B Hardness, Calculation Method: Preparation: Dilution: Date Analyzed: Date Prepared: SM 2340B N/A 1.0 03/03/2009 1527 N/A Analysis Batch: 660-75708 Analyte Result (mg/L) Hardness as calcium carbonate Calcium hardness as calcium carbonate Magnesium hardness as calcium carbonate 420 400 15 TestAmerica Tampa Page 144 of 221 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier No Equipment N/A 1.0 mL PQL PQL 3.3 1.2 2.1 3.3 1.2 2.1 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-L_022509 Lab Sample ID: Client Matrix: 660-27893-44 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1105 02/26/2009 1030 6010B Metals (ICP)-Total Recoverable Method: Preparation: Dilution: Date Analyzed: Date Prepared: 6010B 3005A 1.0 03/03/2009 1420 02/27/2009 1027 Analysis Batch: 660-75689 Prep Batch: 660-75517 Analyte Result (mg/L) Calcium Iron Potassium Magnesium Manganese Sodium 78 4.2 0.35 1.9 0.0052 17 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier I TJA ICP TRACE 9C03A 50 mL 50 mL MDL PQL 0.10 0.050 0.19 0.020 0.0010 0.31 0.50 0.20 1.0 0.080 0.0040 0.50 6010B Metals (ICP)-Dissolved Method: Preparation: Dilution: Date Analyzed: Date Prepared: 6010B 3005A 1.0 03/03/2009 1437 02/27/2009 1027 Analysis Batch: 660-75689 Prep Batch: 660-75517 Analyte Result (mg/L) Iron, Dissolved Manganese, Dissolved 4.0 0.0051 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier TJA ICP TRACE 9C03A 50 mL 50 mL MDL PQL 0.050 0.0010 0.20 0.0040 SM 2340B Hardness, Calculation Method: Preparation: Dilution: Date Analyzed: Date Prepared: SM 2340B N/A 1.0 03/03/2009 1527 N/A Analysis Batch: 660-75708 Analyte Result (mg/L) Hardness as calcium carbonate Calcium hardness as calcium carbonate Magnesium hardness as calcium carbonate 200 190 7.9 TestAmerica Tampa Page 145 of 221 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier No Equipment N/A 1.0 mL PQL PQL 3.3 1.2 2.1 3.3 1.2 2.1 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-I_022509 Lab Sample ID: Client Matrix: 660-27893-45 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/25/2009 1440 02/26/2009 1030 6010B Metals (ICP)-Total Recoverable Method: Preparation: Dilution: Date Analyzed: Date Prepared: 6010B 3005A 1.0 03/03/2009 1443 02/27/2009 1027 Analysis Batch: 660-75689 Prep Batch: 660-75517 Analyte Result (mg/L) Calcium Iron Potassium Magnesium Manganese Sodium 93 2.5 0.50 2.8 0.0051 14 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier I TJA ICP TRACE 9C03A 50 mL 50 mL MDL PQL 0.10 0.050 0.19 0.020 0.0010 0.31 0.50 0.20 1.0 0.080 0.0040 0.50 6010B Metals (ICP)-Dissolved Method: Preparation: Dilution: Date Analyzed: Date Prepared: 6010B 3005A 1.0 03/03/2009 1448 02/27/2009 1027 Analysis Batch: 660-75689 Prep Batch: 660-75517 Analyte Result (mg/L) Iron, Dissolved Manganese, Dissolved 2.2 0.0068 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier TJA ICP TRACE 9C03A 50 mL 50 mL MDL PQL 0.050 0.0010 0.20 0.0040 SM 2340B Hardness, Calculation Method: Preparation: Dilution: Date Analyzed: Date Prepared: SM 2340B N/A 1.0 03/03/2009 1527 N/A Analysis Batch: 660-75708 Analyte Result (mg/L) Hardness as calcium carbonate Calcium hardness as calcium carbonate Magnesium hardness as calcium carbonate 240 230 11 TestAmerica Tampa Page 146 of 221 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier No Equipment N/A 1.0 mL PQL PQL 3.3 1.2 2.1 3.3 1.2 2.1 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-C_022609 Lab Sample ID: Client Matrix: 660-27893-46 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/26/2009 0755 02/26/2009 1030 6010B Metals (ICP)-Total Recoverable Method: Preparation: Dilution: Date Analyzed: Date Prepared: 6010B 3005A 1.0 03/03/2009 1454 02/27/2009 1027 Analysis Batch: 660-75689 Prep Batch: 660-75517 Analyte Result (mg/L) Calcium Iron Potassium Magnesium Manganese Sodium 100 3.5 0.54 2.1 0.025 13 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier I TJA ICP TRACE 9C03A 50 mL 50 mL MDL PQL 0.10 0.050 0.19 0.020 0.0010 0.31 0.50 0.20 1.0 0.080 0.0040 0.50 6010B Metals (ICP)-Dissolved Method: Preparation: Dilution: Date Analyzed: Date Prepared: 6010B 3005A 1.0 03/03/2009 1500 02/27/2009 1027 Analysis Batch: 660-75689 Prep Batch: 660-75517 Analyte Result (mg/L) Iron, Dissolved Manganese, Dissolved 3.4 0.023 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier TJA ICP TRACE 9C03A 50 mL 50 mL MDL PQL 0.050 0.0010 0.20 0.0040 SM 2340B Hardness, Calculation Method: Preparation: Dilution: Date Analyzed: Date Prepared: SM 2340B N/A 1.0 03/03/2009 1527 N/A Analysis Batch: 660-75708 Analyte Result (mg/L) Hardness as calcium carbonate Calcium hardness as calcium carbonate Magnesium hardness as calcium carbonate 260 250 8.7 TestAmerica Tampa Page 147 of 221 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier No Equipment N/A 1.0 mL PQL PQL 3.3 1.2 2.1 3.3 1.2 2.1 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IDPT-9_022609 Lab Sample ID: Client Matrix: 660-27893-47 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/26/2009 0745 02/26/2009 1030 6010B Metals (ICP)-Total Recoverable Method: Preparation: Dilution: Date Analyzed: Date Prepared: 6010B 3005A 1.0 03/03/2009 1505 02/27/2009 1027 Analysis Batch: 660-75689 Prep Batch: 660-75517 Analyte Result (mg/L) Calcium Iron Potassium Magnesium Manganese Sodium 46 7.2 1.4 5.6 0.0089 19 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier TJA ICP TRACE 9C03A 50 mL 50 mL MDL PQL 0.10 0.050 0.19 0.020 0.0010 0.31 0.50 0.20 1.0 0.080 0.0040 0.50 6010B Metals (ICP)-Dissolved Method: Preparation: Dilution: Date Analyzed: Date Prepared: 6010B 3005A 1.0 03/03/2009 1511 02/27/2009 1027 Analysis Batch: 660-75689 Prep Batch: 660-75517 Analyte Result (mg/L) Iron, Dissolved Manganese, Dissolved 3.3 0.0060 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier TJA ICP TRACE 9C03A 50 mL 50 mL MDL PQL 0.050 0.0010 0.20 0.0040 SM 2340B Hardness, Calculation Method: Preparation: Dilution: Date Analyzed: Date Prepared: SM 2340B N/A 1.0 03/03/2009 1527 N/A Analysis Batch: 660-75708 Analyte Result (mg/L) Hardness as calcium carbonate Calcium hardness as calcium carbonate Magnesium hardness as calcium carbonate 140 110 23 TestAmerica Tampa Page 148 of 221 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier No Equipment N/A 1.0 mL PQL PQL 3.3 1.2 2.1 3.3 1.2 2.1 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IDPT-15_022609 Lab Sample ID: Client Matrix: 660-27893-48 Water Job Number: 660-27893-1 Date Sampled: Date Received: 02/26/2009 0805 02/26/2009 1030 6010B Metals (ICP)-Total Recoverable Method: Preparation: Dilution: Date Analyzed: Date Prepared: 6010B 3005A 1.0 03/03/2009 1517 02/27/2009 1027 Analysis Batch: 660-75689 Prep Batch: 660-75517 Analyte Result (mg/L) Calcium Iron Potassium Magnesium Manganese Sodium 61 9.6 1.0 2.5 0.011 27 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier TJA ICP TRACE 9C03A 50 mL 50 mL MDL PQL 0.10 0.050 0.19 0.020 0.0010 0.31 0.50 0.20 1.0 0.080 0.0040 0.50 6010B Metals (ICP)-Dissolved Method: Preparation: Dilution: Date Analyzed: Date Prepared: 6010B 3005A 1.0 03/03/2009 1523 02/27/2009 1027 Analysis Batch: 660-75689 Prep Batch: 660-75517 Analyte Result (mg/L) Iron, Dissolved Manganese, Dissolved 11 0.012 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier TJA ICP TRACE 9C03A 50 mL 50 mL MDL PQL 0.050 0.0010 0.20 0.0040 SM 2340B Hardness, Calculation Method: Preparation: Dilution: Date Analyzed: Date Prepared: SM 2340B N/A 1.0 03/03/2009 1527 N/A Analysis Batch: 660-75708 Analyte Result (mg/L) Hardness as calcium carbonate Calcium hardness as calcium carbonate Magnesium hardness as calcium carbonate 160 150 10 TestAmerica Tampa Page 149 of 221 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier No Equipment N/A 1.0 mL PQL PQL 3.3 1.2 2.1 3.3 1.2 2.1 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 General Chemistry TestAmerica Tampa Page 150 of 221 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 General Chemistry Client Sample ID: Lab Sample ID: Client Matrix: IDPT-14_022509 660-27893-41 Water Analyte Total Dissolved Solids Date Sampled: Date Received: Result 580 Anly Batch: 640-54348 Units mg/L Date Analyzed MDL 10 02/27/2009 1212 PQL 10 Dil 1.0 Method SM 2540C Total Suspended Solids 65 Anly Batch: 640-54352 mg/L Date Analyzed 2.4 02/27/2009 1228 5.0 1.0 SM 2540D Bromide 0.54 Anly Batch: 660-75752 mg/L Date Analyzed 0.027 03/02/2009 1809 0.050 1.0 300.0 Sulfate 36 Anly Batch: 660-75752 J3 mg/L Date Analyzed 0.20 03/04/2009 1425 0.50 1.0 300.0 Chloride 170 Anly Batch: 660-75752 J3 mg/L Date Analyzed 0.40 03/04/2009 1437 1.0 2.0 300.0 Nitrite as N 0.10 Anly Batch: 660-75441 U mg/L Date Analyzed 0.10 02/26/2009 1531 0.50 1.0 353.2 Nitrate Nitrite as N 0.10 Anly Batch: 660-75644 1.0 353.2 0.10 Anly Batch: 660-75441 0.10 03/02/2009 1303 03/02/2009 1303 0.10 02/26/2009 1531 0.50 Nitrate as N U mg/L Date Analyzed Date Prepared: U mg/L Date Analyzed 0.50 1.0 353.2 Chemical Oxygen Demand 23 Anly Batch: 660-75563 Prep Batch: 660-75561 Total Organic Carbon 8.7 Anly Batch: 660-75675 mg/L Date Analyzed Date Prepared: mg/L Date Analyzed 10 02/27/2009 1500 02/27/2009 1220 1.1 03/02/2009 2023 20 1.0 SM 5220D 2.0 2.0 SM 5310C TestAmerica Tampa Qual 02/25/2009 1317 02/26/2009 1030 Page 151 of 221 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 General Chemistry Client Sample ID: Lab Sample ID: Client Matrix: IDPT-14_022509 660-27893-41 Water Analyte Alkalinity Date Sampled: Date Received: Result 150 Anly Batch: 660-75553 Units mg/L Date Analyzed PQL 1.0 02/27/2009 1232 PQL 1.0 Dil 1.0 Method SM 2320B Bicarbonate Alkalinity as CaCO3 150 Anly Batch: 660-75553 mg/L Date Analyzed 1.0 02/27/2009 1232 1.0 1.0 SM 2320B Carbonate Alkalinity as CaCO3 1.0 Anly Batch: 660-75553 U mg/L Date Analyzed 1.0 02/27/2009 1232 1.0 1.0 SM 2320B Hydroxide Alkalinity 1.0 Anly Batch: 660-75553 U mg/L Date Analyzed 1.0 02/27/2009 1232 1.0 1.0 SM 2320B Phenolphthalein Alkalinity 1.0 Anly Batch: 660-75553 U mg/L Date Analyzed 1.0 02/27/2009 1232 1.0 1.0 SM 2320B TestAmerica Tampa Qual 02/25/2009 1317 02/26/2009 1030 Page 152 of 221 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 General Chemistry Client Sample ID: Lab Sample ID: Client Matrix: DMW-F_022509 660-27893-42 Water Analyte Total Dissolved Solids Date Sampled: Date Received: Result 360 Anly Batch: 640-54348 Units mg/L Date Analyzed MDL 10 02/27/2009 1212 PQL 10 Dil 1.0 Method SM 2540C Total Suspended Solids 12 Anly Batch: 640-54352 mg/L Date Analyzed 0.49 02/27/2009 1228 1.0 1.0 SM 2540D Bromide 0.13 Anly Batch: 660-75752 mg/L Date Analyzed 0.027 03/02/2009 1926 0.050 1.0 300.0 Chloride 40 Anly Batch: 660-75752 mg/L Date Analyzed 0.20 03/04/2009 1515 0.50 1.0 300.0 Sulfate 19 Anly Batch: 660-75752 mg/L Date Analyzed 0.20 03/04/2009 1515 0.50 1.0 300.0 Nitrite as N 0.10 Anly Batch: 660-75441 U mg/L Date Analyzed 0.10 02/26/2009 1531 0.50 1.0 353.2 Nitrate Nitrite as N 0.10 Anly Batch: 660-75644 1.0 353.2 0.10 Anly Batch: 660-75441 0.10 03/02/2009 1303 03/02/2009 1303 0.10 02/26/2009 1531 0.50 Nitrate as N U mg/L Date Analyzed Date Prepared: U mg/L Date Analyzed 0.50 1.0 353.2 Chemical Oxygen Demand 14 Anly Batch: 660-75563 Prep Batch: 660-75561 Total Organic Carbon 5.8 Anly Batch: 660-75675 I mg/L Date Analyzed Date Prepared: mg/L Date Analyzed 10 02/27/2009 1500 02/27/2009 1220 0.53 03/02/2009 2046 20 1.0 SM 5220D 1.0 1.0 SM 5310C TestAmerica Tampa Qual 02/25/2009 0828 02/26/2009 1030 Page 153 of 221 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 General Chemistry Client Sample ID: Lab Sample ID: Client Matrix: DMW-F_022509 660-27893-42 Water Analyte Alkalinity Date Sampled: Date Received: Result 230 Anly Batch: 660-75553 Units mg/L Date Analyzed PQL 1.0 02/27/2009 1239 PQL 1.0 Dil 1.0 Method SM 2320B Bicarbonate Alkalinity as CaCO3 230 Anly Batch: 660-75553 mg/L Date Analyzed 1.0 02/27/2009 1239 1.0 1.0 SM 2320B Carbonate Alkalinity as CaCO3 1.0 Anly Batch: 660-75553 U mg/L Date Analyzed 1.0 02/27/2009 1239 1.0 1.0 SM 2320B Hydroxide Alkalinity 1.0 Anly Batch: 660-75553 U mg/L Date Analyzed 1.0 02/27/2009 1239 1.0 1.0 SM 2320B Phenolphthalein Alkalinity 1.0 Anly Batch: 660-75553 U mg/L Date Analyzed 1.0 02/27/2009 1239 1.0 1.0 SM 2320B TestAmerica Tampa Qual 02/25/2009 0828 02/26/2009 1030 Page 154 of 221 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 General Chemistry Client Sample ID: Lab Sample ID: Client Matrix: DMW-J_022509 660-27893-43 Water Analyte Total Dissolved Solids Date Sampled: Date Received: Result 780 Anly Batch: 640-54348 Units mg/L Date Analyzed MDL 10 02/27/2009 1212 PQL 10 Dil 1.0 Method SM 2540C Total Suspended Solids 27 Anly Batch: 640-54352 mg/L Date Analyzed 0.53 02/27/2009 1228 1.1 1.0 SM 2540D Bromide 0.47 Anly Batch: 660-75752 mg/L Date Analyzed 0.027 03/02/2009 1952 0.050 1.0 300.0 Sulfate 54 Anly Batch: 660-75752 mg/L Date Analyzed 0.20 03/04/2009 1527 0.50 1.0 300.0 Chloride 270 Anly Batch: 660-75752 mg/L Date Analyzed 0.80 03/04/2009 1540 2.0 4.0 300.0 Nitrite as N 0.10 Anly Batch: 660-75441 U mg/L Date Analyzed 0.10 02/26/2009 1531 0.50 1.0 353.2 Nitrate Nitrite as N 0.10 Anly Batch: 660-75644 1.0 353.2 0.10 Anly Batch: 660-75441 0.10 03/02/2009 1303 03/02/2009 1303 0.10 02/26/2009 1531 0.50 Nitrate as N U mg/L Date Analyzed Date Prepared: U mg/L Date Analyzed 0.50 1.0 353.2 Chemical Oxygen Demand 14 Anly Batch: 660-75563 Prep Batch: 660-75561 Total Organic Carbon 5.5 Anly Batch: 660-75675 I mg/L Date Analyzed Date Prepared: mg/L Date Analyzed 10 02/27/2009 1500 02/27/2009 1220 0.53 03/02/2009 2113 20 1.0 SM 5220D 1.0 1.0 SM 5310C TestAmerica Tampa Qual 02/25/2009 1216 02/26/2009 1030 Page 155 of 221 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 General Chemistry Client Sample ID: Lab Sample ID: Client Matrix: DMW-J_022509 660-27893-43 Water Analyte Alkalinity Date Sampled: Date Received: Result 180 Anly Batch: 660-75553 Units mg/L Date Analyzed PQL 1.0 02/27/2009 1245 PQL 1.0 Dil 1.0 Method SM 2320B Bicarbonate Alkalinity as CaCO3 180 Anly Batch: 660-75553 mg/L Date Analyzed 1.0 02/27/2009 1245 1.0 1.0 SM 2320B Carbonate Alkalinity as CaCO3 1.0 Anly Batch: 660-75553 U mg/L Date Analyzed 1.0 02/27/2009 1245 1.0 1.0 SM 2320B Hydroxide Alkalinity 1.0 Anly Batch: 660-75553 U mg/L Date Analyzed 1.0 02/27/2009 1245 1.0 1.0 SM 2320B Phenolphthalein Alkalinity 1.0 Anly Batch: 660-75553 U mg/L Date Analyzed 1.0 02/27/2009 1245 1.0 1.0 SM 2320B TestAmerica Tampa Qual 02/25/2009 1216 02/26/2009 1030 Page 156 of 221 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 General Chemistry Client Sample ID: Lab Sample ID: Client Matrix: DMW-L_022509 660-27893-44 Water Analyte Total Dissolved Solids Date Sampled: Date Received: Result 270 Anly Batch: 640-54348 Units mg/L Date Analyzed MDL 5.0 02/27/2009 1212 PQL 5.0 Dil 1.0 Method SM 2540C Total Suspended Solids 26 Anly Batch: 640-54352 mg/L Date Analyzed 0.80 02/27/2009 1228 1.7 1.0 SM 2540D Bromide 0.027 Anly Batch: 660-75752 U mg/L Date Analyzed 0.027 03/02/2009 2018 0.050 1.0 300.0 Chloride 35 Anly Batch: 660-75752 mg/L Date Analyzed 0.20 03/04/2009 1552 0.50 1.0 300.0 Sulfate 8.6 Anly Batch: 660-75752 mg/L Date Analyzed 0.20 03/04/2009 1552 0.50 1.0 300.0 Nitrite as N 0.10 Anly Batch: 660-75441 U mg/L Date Analyzed 0.10 02/26/2009 1531 0.50 1.0 353.2 Nitrate Nitrite as N 0.10 Anly Batch: 660-75644 1.0 353.2 0.10 Anly Batch: 660-75441 0.10 03/02/2009 1303 03/02/2009 1303 0.10 02/26/2009 1531 0.50 Nitrate as N U mg/L Date Analyzed Date Prepared: U mg/L Date Analyzed 0.50 1.0 353.2 Chemical Oxygen Demand 10 Anly Batch: 660-75563 Prep Batch: 660-75561 Total Organic Carbon 3.0 Anly Batch: 660-75675 U mg/L Date Analyzed Date Prepared: mg/L Date Analyzed 10 02/27/2009 1500 02/27/2009 1220 0.53 03/02/2009 2231 20 1.0 SM 5220D 1.0 1.0 SM 5310C TestAmerica Tampa Qual 02/25/2009 1105 02/26/2009 1030 Page 157 of 221 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 General Chemistry Client Sample ID: Lab Sample ID: Client Matrix: DMW-L_022509 660-27893-44 Water Analyte Alkalinity Date Sampled: Date Received: Result 200 Anly Batch: 660-75553 Units mg/L Date Analyzed PQL 1.0 02/27/2009 1303 PQL 1.0 Dil 1.0 Method SM 2320B Bicarbonate Alkalinity as CaCO3 200 Anly Batch: 660-75553 mg/L Date Analyzed 1.0 02/27/2009 1303 1.0 1.0 SM 2320B Carbonate Alkalinity as CaCO3 1.0 Anly Batch: 660-75553 U mg/L Date Analyzed 1.0 02/27/2009 1303 1.0 1.0 SM 2320B Hydroxide Alkalinity 1.0 Anly Batch: 660-75553 U mg/L Date Analyzed 1.0 02/27/2009 1303 1.0 1.0 SM 2320B Phenolphthalein Alkalinity 1.0 Anly Batch: 660-75553 U mg/L Date Analyzed 1.0 02/27/2009 1303 1.0 1.0 SM 2320B TestAmerica Tampa Qual 02/25/2009 1105 02/26/2009 1030 Page 158 of 221 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 General Chemistry Client Sample ID: Lab Sample ID: Client Matrix: DMW-I_022509 660-27893-45 Water Analyte Total Dissolved Solids Date Sampled: Date Received: Result 340 Anly Batch: 640-54348 Units mg/L Date Analyzed MDL 10 02/27/2009 1212 PQL 10 Dil 1.0 Method SM 2540C Total Suspended Solids 32 Anly Batch: 640-54352 mg/L Date Analyzed 0.80 02/27/2009 1228 1.7 1.0 SM 2540D Bromide 0.22 Anly Batch: 660-75752 mg/L Date Analyzed 0.027 03/02/2009 2044 0.050 1.0 300.0 Chloride 75 Anly Batch: 660-75752 mg/L Date Analyzed 0.20 03/04/2009 1605 0.50 1.0 300.0 Sulfate 2.0 Anly Batch: 660-75752 mg/L Date Analyzed 0.20 03/04/2009 1605 0.50 1.0 300.0 Nitrite as N 0.10 Anly Batch: 660-75441 U mg/L Date Analyzed 0.10 02/26/2009 1531 0.50 1.0 353.2 Nitrate Nitrite as N 0.10 Anly Batch: 660-75644 1.0 353.2 0.10 Anly Batch: 660-75441 0.10 03/02/2009 1303 03/02/2009 1303 0.10 02/26/2009 1531 0.50 Nitrate as N U mg/L Date Analyzed Date Prepared: U mg/L Date Analyzed 0.50 1.0 353.2 Chemical Oxygen Demand 26 Anly Batch: 660-75563 Prep Batch: 660-75561 Total Organic Carbon 8.7 Anly Batch: 660-75675 mg/L Date Analyzed Date Prepared: mg/L Date Analyzed 10 02/27/2009 1500 02/27/2009 1220 0.53 03/02/2009 2255 20 1.0 SM 5220D 1.0 1.0 SM 5310C TestAmerica Tampa Qual 02/25/2009 1440 02/26/2009 1030 Page 159 of 221 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 General Chemistry Client Sample ID: Lab Sample ID: Client Matrix: DMW-I_022509 660-27893-45 Water Analyte Alkalinity Date Sampled: Date Received: Result 180 Anly Batch: 660-75553 Units mg/L Date Analyzed PQL 1.0 02/27/2009 1309 PQL 1.0 Dil 1.0 Method SM 2320B Bicarbonate Alkalinity as CaCO3 180 Anly Batch: 660-75553 mg/L Date Analyzed 1.0 02/27/2009 1309 1.0 1.0 SM 2320B Carbonate Alkalinity as CaCO3 1.0 Anly Batch: 660-75553 U mg/L Date Analyzed 1.0 02/27/2009 1309 1.0 1.0 SM 2320B Hydroxide Alkalinity 1.0 Anly Batch: 660-75553 U mg/L Date Analyzed 1.0 02/27/2009 1309 1.0 1.0 SM 2320B Phenolphthalein Alkalinity 1.0 Anly Batch: 660-75553 U mg/L Date Analyzed 1.0 02/27/2009 1309 1.0 1.0 SM 2320B TestAmerica Tampa Qual 02/25/2009 1440 02/26/2009 1030 Page 160 of 221 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 General Chemistry Client Sample ID: Lab Sample ID: Client Matrix: DMW-C_022609 660-27893-46 Water Analyte Total Dissolved Solids Date Sampled: Date Received: Result 320 Anly Batch: 640-54348 Units mg/L Date Analyzed MDL 10 02/27/2009 1212 PQL 10 Dil 1.0 Method SM 2540C Total Suspended Solids 3.9 Anly Batch: 640-54352 mg/L Date Analyzed 0.48 02/27/2009 1228 1.0 1.0 SM 2540D Bromide 0.027 Anly Batch: 660-75752 U mg/L Date Analyzed 0.027 03/02/2009 2110 0.050 1.0 300.0 Chloride 41 Anly Batch: 660-75752 mg/L Date Analyzed 0.20 03/04/2009 1617 0.50 1.0 300.0 Sulfate 71 Anly Batch: 660-75752 mg/L Date Analyzed 0.20 03/04/2009 1617 0.50 1.0 300.0 Nitrite as N 0.10 Anly Batch: 660-75441 U mg/L Date Analyzed 0.10 02/26/2009 1531 0.50 1.0 353.2 Nitrate Nitrite as N 0.10 Anly Batch: 660-75644 1.0 353.2 0.10 Anly Batch: 660-75441 0.10 03/02/2009 1303 03/02/2009 1303 0.10 02/26/2009 1531 0.50 Nitrate as N U mg/L Date Analyzed Date Prepared: U mg/L Date Analyzed 0.50 1.0 353.2 Chemical Oxygen Demand 10 Anly Batch: 660-75563 Prep Batch: 660-75561 Total Organic Carbon 6.8 Anly Batch: 660-75675 U mg/L Date Analyzed Date Prepared: mg/L Date Analyzed 10 02/27/2009 1500 02/27/2009 1220 0.53 03/02/2009 2318 20 1.0 SM 5220D 1.0 1.0 SM 5310C TestAmerica Tampa Qual 02/26/2009 0755 02/26/2009 1030 Page 161 of 221 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 General Chemistry Client Sample ID: Lab Sample ID: Client Matrix: DMW-C_022609 660-27893-46 Water Analyte Alkalinity Date Sampled: Date Received: Result 130 Anly Batch: 660-75553 Units mg/L Date Analyzed PQL 1.0 02/27/2009 1316 PQL 1.0 Dil 1.0 Method SM 2320B Bicarbonate Alkalinity as CaCO3 130 Anly Batch: 660-75553 mg/L Date Analyzed 1.0 02/27/2009 1316 1.0 1.0 SM 2320B Carbonate Alkalinity as CaCO3 1.0 Anly Batch: 660-75553 U mg/L Date Analyzed 1.0 02/27/2009 1316 1.0 1.0 SM 2320B Hydroxide Alkalinity 1.0 Anly Batch: 660-75553 U mg/L Date Analyzed 1.0 02/27/2009 1316 1.0 1.0 SM 2320B Phenolphthalein Alkalinity 1.0 Anly Batch: 660-75553 U mg/L Date Analyzed 1.0 02/27/2009 1316 1.0 1.0 SM 2320B TestAmerica Tampa Qual 02/26/2009 0755 02/26/2009 1030 Page 162 of 221 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 General Chemistry Client Sample ID: Lab Sample ID: Client Matrix: IDPT-9_022609 660-27893-47 Water Analyte Total Dissolved Solids Date Sampled: Date Received: Result 380 Anly Batch: 640-54348 Units mg/L Date Analyzed MDL 5.0 02/27/2009 1212 PQL 5.0 Dil 1.0 Method SM 2540C Total Suspended Solids 500 Anly Batch: 640-54352 mg/L Date Analyzed 9.6 02/27/2009 1228 20 1.0 SM 2540D Bromide 0.29 Anly Batch: 660-75752 mg/L Date Analyzed 0.027 03/02/2009 2227 0.050 1.0 300.0 Chloride 83 Anly Batch: 660-75752 mg/L Date Analyzed 0.20 03/04/2009 1655 0.50 1.0 300.0 Sulfate 8.5 Anly Batch: 660-75752 mg/L Date Analyzed 0.20 03/04/2009 1655 0.50 1.0 300.0 Nitrite as N 1.4 Anly Batch: 660-75441 mg/L Date Analyzed 0.10 02/26/2009 1531 0.50 1.0 353.2 Nitrate Nitrite as N 0.10 Anly Batch: 660-75644 1.0 353.2 0.10 Anly Batch: 660-75441 0.10 03/02/2009 1303 03/02/2009 1303 0.10 02/26/2009 1531 0.50 Nitrate as N U mg/L Date Analyzed Date Prepared: U mg/L Date Analyzed 0.50 1.0 353.2 Chemical Oxygen Demand 45 Anly Batch: 660-75563 Prep Batch: 660-75561 Total Organic Carbon 5.8 Anly Batch: 660-75675 mg/L Date Analyzed Date Prepared: mg/L Date Analyzed 10 02/27/2009 1500 02/27/2009 1220 2.1 03/02/2009 2338 20 1.0 SM 5220D 4.0 4.0 SM 5310C TestAmerica Tampa Qual 02/26/2009 0745 02/26/2009 1030 Page 163 of 221 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 General Chemistry Client Sample ID: Lab Sample ID: Client Matrix: IDPT-9_022609 660-27893-47 Water Analyte Alkalinity Date Sampled: Date Received: Result 61 Anly Batch: 660-75622 Units mg/L Date Analyzed PQL 1.0 03/02/2009 0920 PQL 1.0 Dil 1.0 Method SM 2320B Bicarbonate Alkalinity as CaCO3 61 Anly Batch: 660-75622 mg/L Date Analyzed 1.0 03/02/2009 0920 1.0 1.0 SM 2320B Carbonate Alkalinity as CaCO3 1.0 Anly Batch: 660-75622 U mg/L Date Analyzed 1.0 03/02/2009 0920 1.0 1.0 SM 2320B Hydroxide Alkalinity 1.0 Anly Batch: 660-75622 U mg/L Date Analyzed 1.0 03/02/2009 0920 1.0 1.0 SM 2320B Phenolphthalein Alkalinity 1.0 Anly Batch: 660-75622 U mg/L Date Analyzed 1.0 03/02/2009 0920 1.0 1.0 SM 2320B TestAmerica Tampa Qual 02/26/2009 0745 02/26/2009 1030 Page 164 of 221 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 General Chemistry Client Sample ID: Lab Sample ID: Client Matrix: IDPT-15_022609 660-27893-48 Water Analyte Total Dissolved Solids Date Sampled: Date Received: Result 410 Anly Batch: 640-54348 Units mg/L Date Analyzed MDL 10 02/27/2009 1212 PQL 10 Dil 1.0 Method SM 2540C Total Suspended Solids 22 Anly Batch: 640-54352 mg/L Date Analyzed 0.80 02/27/2009 1228 1.7 1.0 SM 2540D Bromide 0.52 Anly Batch: 660-75752 mg/L Date Analyzed 0.027 03/02/2009 2253 0.050 1.0 300.0 Sulfate 6.1 Anly Batch: 660-75752 mg/L Date Analyzed 0.20 03/04/2009 1707 0.50 1.0 300.0 Chloride 170 Anly Batch: 660-75752 mg/L Date Analyzed 0.80 03/05/2009 0926 2.0 4.0 300.0 Nitrite as N 0.10 Anly Batch: 660-75441 U mg/L Date Analyzed 0.10 02/26/2009 1531 0.50 1.0 353.2 Nitrate Nitrite as N 0.10 Anly Batch: 660-75644 1.0 353.2 0.10 Anly Batch: 660-75441 0.10 03/02/2009 1303 03/02/2009 1303 0.10 02/26/2009 1531 0.50 Nitrate as N U J3 mg/L Date Analyzed Date Prepared: U mg/L Date Analyzed 0.50 1.0 353.2 Chemical Oxygen Demand 11 Anly Batch: 660-75563 Prep Batch: 660-75561 Total Organic Carbon 5.2 Anly Batch: 660-75675 I mg/L Date Analyzed Date Prepared: mg/L Date Analyzed 10 02/27/2009 1500 02/27/2009 1220 0.53 03/03/2009 0006 20 1.0 SM 5220D 1.0 1.0 SM 5310C TestAmerica Tampa Qual 02/26/2009 0805 02/26/2009 1030 Page 165 of 221 04/06/2009 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 General Chemistry Client Sample ID: Lab Sample ID: Client Matrix: IDPT-15_022609 660-27893-48 Water Analyte Alkalinity Date Sampled: Date Received: Result 37 Anly Batch: 660-75622 Units mg/L Date Analyzed PQL 1.0 03/02/2009 0929 PQL 1.0 Dil 1.0 Method SM 2320B Bicarbonate Alkalinity as CaCO3 37 Anly Batch: 660-75622 mg/L Date Analyzed 1.0 03/02/2009 0929 1.0 1.0 SM 2320B Carbonate Alkalinity as CaCO3 1.0 Anly Batch: 660-75622 U mg/L Date Analyzed 1.0 03/02/2009 0929 1.0 1.0 SM 2320B Hydroxide Alkalinity 1.0 Anly Batch: 660-75622 U mg/L Date Analyzed 1.0 03/02/2009 0929 1.0 1.0 SM 2320B Phenolphthalein Alkalinity 1.0 Anly Batch: 660-75622 U mg/L Date Analyzed 1.0 03/02/2009 0929 1.0 1.0 SM 2320B TestAmerica Tampa Qual 02/26/2009 0805 02/26/2009 1030 Page 166 of 221 04/06/2009 DATA REPORTING QUALIFIERS Client: ARCADIS U.S., Inc. Lab Section Job Number: 660-27893-1 Qualifier Description U Indicates that the compound was analyzed for but not detected. I The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. J3 Estimated value; value may not be accurate. Spike recovery or RPD outside of criteria. U Indicates that the compound was analyzed for but not detected. I The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. J3 Estimated value; value may not be accurate. Spike recovery or RPD outside of criteria. U Indicates that the compound was analyzed for but not detected. I The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. GC/MS VOA Metals General Chemistry TestAmerica Tampa Page 167 of 221 04/06/2009 QUALITY CONTROL RESULTS TestAmerica Tampa Page 168 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Surrogate Recovery Report 8260B Volatile Organic Compounds (GC/MS) Client Matrix: Water Lab Sample ID Client Sample ID TOL %Rec BFB %Rec 660-27893-1 DMW-P_022509 101 78 98 660-27893-2 DMW-O_022509 98 77 101 660-27893-3 DMW-Q_022509 116 82 100 660-27893-4 DMW-C_022509 105 89 106 660-27893-5 IMW-D_022509 101 84 95 660-27893-6 DMW-B_022509 105 81 101 660-27893-7 IDPT-15_022509 107 86 103 660-27893-8 DMW-8_022509 104 88 101 660-27893-9 SMW-D_022509 101 79 105 660-27893-10 IDPT-8_022509 92 82 107 660-27893-11 IDPT-9_022509 101 86 108 660-27893-12 SMW-E_022509 99 87 108 660-27893-13 SMW-H_022509 95 86 107 660-27893-14 DMW-N_022509 94 84 110 660-27893-15 DUPE E_022509 103 90 106 660-27893-16 SMW-I_022509 103 87 106 660-27893-17 DMW-I_022509 118 84 107 660-27893-18 SMW-N_022509 103 84 108 660-27893-19 IDPT-12_022509 98 90 109 660-27893-20 IMW-J_022509 101 91 110 660-27893-21 DMW-A_022509 99 100 99 660-27893-22 DMW-W_022509 102 105 98 660-27893-23 H-1_022509 101 100 98 660-27893-24 SMW-A_022509 102 105 101 660-27893-25 Trip Blank 3_022509 101 101 97 660-27893-26 IDPT-1_022509 100 101 100 660-27893-27 IDPT-2_022509 100 102 102 660-27893-28 IDPT-5_022509 100 99 100 660-27893-29 IDPT-6_022509 101 102 104 Surrogate TOL = Toluene-d8 (Surr) BFB = 4-Bromofluorobenzene DBFM = Dibromofluoromethane DBFM %Rec Acceptance Limits 77-122 74-126 70-130 TestAmerica Tampa Page 169 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Surrogate Recovery Report 8260B Volatile Organic Compounds (GC/MS) Client Matrix: Water Lab Sample ID 660-27893-30 Client Sample ID IDPT-10_022509 TOL %Rec 103 BFB %Rec 104 DBFM %Rec 102 660-27893-31 IDPT-13_022509 101 103 101 660-27893-32 IDPT-14_022509 101 102 101 660-27893-33 IMW-F_022509 101 104 102 660-27893-34 DMW-F_022509 103 101 104 660-27893-35 DMW-J_022509 99 101 98 660-27893-36 DMW-K_022509 101 102 98 660-27893-37 DMW-L_022509 103 104 100 660-27893-38 DUPE D_022509 100 101 100 660-27893-39 DUPE H_022509 102 102 101 660-27893-40 Trip Blank_022509 102 106 98 MB 660-75524/2 93 87 102 MB 660-75614/2 94 83 107 MB 660-75683/2 114 87 107 MB 660-75698/2 98 101 95 MB 660-75699/2 99 102 96 MB 660-75700/2 102 106 100 LCS 660-75524/1 91 85 99 LCS 660-75614/1 92 85 108 LCS 660-75683/1 92 88 106 LCS 660-75698/1 100 100 96 LCS 660-75699/1 99 100 95 102 105 102 88 85 105 LCS 660-75700/1 660-27893-14 MS DMW-N_022509 MS 660-27893-21 MS DMW-A_022509 MS 98 100 97 660-27893-22 MS DMW-W_022509 MS 101 103 100 660-27893-26 MS IDPT-1_022509 MS 100 100 98 660-27890-C-3 MS 92 81 98 660-27916-D-15 MS 94 89 104 Surrogate TOL = Toluene-d8 (Surr) BFB = 4-Bromofluorobenzene DBFM = Dibromofluoromethane Acceptance Limits 77-122 74-126 70-130 TestAmerica Tampa Page 170 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Surrogate Recovery Report 8260B Volatile Organic Compounds (GC/MS) Client Matrix: Water Lab Sample ID 660-27893-14 MSD 660-27893-21 MSD 660-27893-22 MSD 660-27893-26 MSD Client Sample ID DMW-N_022509 MSD DMW-A_022509 MSD DMW-W_022509 MSD IDPT-1_022509 MSD TOL %Rec 90 BFB %Rec 82 DBFM %Rec 104 98 103 96 102 104 101 100 101 100 660-27890-D-3 MSD 94 82 99 660-27916-B-13 DU 86 83 106 Surrogate TOL = Toluene-d8 (Surr) BFB = 4-Bromofluorobenzene DBFM = Dibromofluoromethane Acceptance Limits 77-122 74-126 70-130 TestAmerica Tampa Page 171 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Method Blank - Batch: 660-75524 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-75524/2 Water 1.0 02/27/2009 1200 02/27/2009 1200 Method: 8260B Preparation: 5030B Analysis Batch: 660-75524 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HB2713.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 172 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Method Blank - Batch: 660-75524 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-75524/2 Water 1.0 02/27/2009 1200 02/27/2009 1200 Method: 8260B Preparation: 5030B Analysis Batch: 660-75524 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HB2713.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene 0.59 0.98 0.63 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 U U U U U U U U U U U U U U U U U U U U U U U U 0.59 0.98 0.63 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 1.0 2.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane % Rec Acceptance Limits 93 87 102 77 - 122 74 - 126 70 - 130 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 173 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Lab Control Spike - Batch: 660-75524 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: LCS 660-75524/1 Water 1.0 02/27/2009 1052 02/27/2009 1052 Method: 8260B Preparation: 5030B Analysis Batch: 660-75524 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HB2709.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Spike Amount Result % Rec. Limit Qual Benzene Chlorobenzene 1,1-Dichloroethene Toluene Trichloroethene 50.0 50.0 50.0 50.0 50.0 52.0 46.8 68.8 47.5 51.7 104 94 138 95 103 62 - 135 72 - 127 46 - 147 68 - 131 56 - 143 Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 660-75524 Method: 8260B Preparation: 5030B MS Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27890-C-3 MS Water 1.0 02/27/2009 1525 02/27/2009 1525 Analysis Batch: 660-75524 Prep Batch: N/A Instrument ID: BVMH GC/MS Lab File ID: 1HB2725.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL MSD Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27890-D-3 MSD Water 1.0 02/27/2009 1542 02/27/2009 1542 Analysis Batch: 660-75524 Prep Batch: N/A Instrument ID: BVMH GC/MS Lab File ID: 1HB2726.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte MS Benzene Chlorobenzene 1,1-Dichloroethene Toluene Trichloroethene 107 103 100 96 103 % Rec. MSD 99 96 86 92 96 Limit RPD RPD Limit 62 - 135 72 - 127 46 - 147 68 - 131 56 - 143 8 7 15 4 8 37 22 30 33 35 MS Qual MSD Qual Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 174 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Method Blank - Batch: 660-75614 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-75614/2 Water 1.0 03/02/2009 1138 03/02/2009 1138 Method: 8260B Preparation: 5030B Analysis Batch: 660-75614 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HC0212.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 175 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Method Blank - Batch: 660-75614 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-75614/2 Water 1.0 03/02/2009 1138 03/02/2009 1138 Method: 8260B Preparation: 5030B Analysis Batch: 660-75614 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HC0212.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene 0.59 0.98 0.63 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 U U U U U U U U U U U U U U U U U U U U U U U U 0.59 0.98 0.63 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 1.0 2.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane % Rec Acceptance Limits 94 83 107 77 - 122 74 - 126 70 - 130 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 176 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Lab Control Spike - Batch: 660-75614 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: LCS 660-75614/1 Water 1.0 03/02/2009 1046 03/02/2009 1046 Method: 8260B Preparation: 5030B Analysis Batch: 660-75614 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HC0209.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Spike Amount Result % Rec. Limit Qual Benzene Chlorobenzene 1,1-Dichloroethene Toluene Trichloroethene 50.0 50.0 50.0 50.0 50.0 53.6 46.4 55.2 47.6 60.0 107 93 110 95 120 62 - 135 72 - 127 46 - 147 68 - 131 56 - 143 Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 660-75614 Method: 8260B Preparation: 5030B MS Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27893-14 Water 1.0 03/02/2009 1756 03/02/2009 1756 Analysis Batch: 660-75614 Prep Batch: N/A Instrument ID: BVMH GC/MS Lab File ID: 1HC0234.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL MSD Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27893-14 Water 1.0 03/02/2009 1813 03/02/2009 1813 Analysis Batch: 660-75614 Prep Batch: N/A Instrument ID: BVMH GC/MS Lab File ID: 1HC0235.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte MS Benzene Chlorobenzene 1,1-Dichloroethene Toluene Trichloroethene 107 98 109 95 117 % Rec. MSD 95 92 97 85 101 Limit RPD RPD Limit 62 - 135 72 - 127 46 - 147 68 - 131 56 - 143 12 6 11 11 14 37 22 30 33 35 MS Qual MSD Qual Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 177 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Method Blank - Batch: 660-75683 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-75683/2 Water 1.0 03/03/2009 1212 03/03/2009 1212 Method: 8260B Preparation: 5030B Analysis Batch: 660-75683 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HC0313.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 178 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Method Blank - Batch: 660-75683 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-75683/2 Water 1.0 03/03/2009 1212 03/03/2009 1212 Method: 8260B Preparation: 5030B Analysis Batch: 660-75683 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HC0313.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene 0.59 0.98 0.63 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 U U U U U U U U U U U U U U U U U U U U U U U U 0.59 0.98 0.63 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 1.0 2.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane % Rec Acceptance Limits 114 87 107 77 - 122 74 - 126 70 - 130 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 179 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Lab Control Spike - Batch: 660-75683 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: LCS 660-75683/1 Water 1.0 03/03/2009 1103 03/03/2009 1103 Method: 8260B Preparation: 5030B Analysis Batch: 660-75683 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HC0309.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Spike Amount Result % Rec. Limit Benzene Chlorobenzene 1,1-Dichloroethene Toluene Trichloroethene 50.0 50.0 50.0 50.0 50.0 50.6 46.1 54.7 46.3 56.1 101 92 109 93 112 62 - 135 72 - 127 46 - 147 68 - 131 56 - 143 Matrix Spike - Batch: 660-75683 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27916-D-15 MS Water 1.0 03/03/2009 1429 03/03/2009 1429 Qual Method: 8260B Preparation: 5030B Analysis Batch: 660-75683 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HC0321.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Sample Result/Qual Spike Amount Result % Rec. Benzene Chlorobenzene 1,1-Dichloroethene Toluene Trichloroethene 0.50 0.63 0.45 0.51 0.50 50.0 50.0 50.0 50.0 50.0 48.1 43.4 50.5 43.6 51.9 96 87 101 87 104 U U U U U Limit Qual 62 - 135 72 - 127 46 - 147 68 - 131 56 - 143 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 180 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Duplicate - Batch: 660-75683 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27916-B-13 DU Water 1.0 03/03/2009 1355 03/03/2009 1355 Method: 8260B Preparation: 5030B Analysis Batch: 660-75683 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HC0319.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Sample Result/Qual Result RPD Limit Qual Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC 37 35 33 28 31 33 33 34 34 38 22 34 20 44 39 25 31 30 40 40 39 29 31 34 47 23 30 28 22 24 40 21 37 21 24 18 29 36 34 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 181 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Duplicate - Batch: 660-75683 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27916-B-13 DU Water 1.0 03/03/2009 1355 03/03/2009 1355 Method: 8260B Preparation: 5030B Analysis Batch: 660-75683 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HC0319.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Sample Result/Qual Result RPD Limit Qual Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene 4.0 2.5 0.59 0.98 0.63 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 4.0 2.5 0.59 0.98 0.63 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC 50 50 34 28 20 22 24 33 65 57 27 21 35 21 26 20 48 21 30 52 31 42 23 36 38 30 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U Surrogate % Rec Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane 86 83 106 Acceptance Limits 77 - 122 74 - 126 70 - 130 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 182 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Method Blank - Batch: 660-75698 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-75698/2 Water 1.0 02/28/2009 0051 02/28/2009 0051 Method: 8260B Preparation: 5030B Analysis Batch: 660-75698 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JB2727.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 183 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Method Blank - Batch: 660-75698 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-75698/2 Water 1.0 02/28/2009 0051 02/28/2009 0051 Method: 8260B Preparation: 5030B Analysis Batch: 660-75698 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JB2727.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene 0.59 0.98 0.63 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 U U U U U U U U U U U U U U U U U U U U U U U U 0.59 0.98 0.63 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 1.0 2.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane % Rec Acceptance Limits 98 101 95 77 - 122 74 - 126 70 - 130 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 184 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Lab Control Spike - Batch: 660-75698 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: LCS 660-75698/1 Water 1.0 02/28/2009 0026 02/28/2009 0026 Method: 8260B Preparation: 5030B Analysis Batch: 660-75698 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JB2726.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Spike Amount Result % Rec. Limit Qual Benzene Chlorobenzene 1,1-Dichloroethene Toluene Trichloroethene 50.0 50.0 50.0 50.0 50.0 53.6 53.5 53.6 54.2 54.2 107 107 107 108 108 62 - 135 72 - 127 46 - 147 68 - 131 56 - 143 Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 660-75698 Method: 8260B Preparation: 5030B MS Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27893-21 Water 1.0 02/28/2009 0205 02/28/2009 0205 Analysis Batch: 660-75698 Prep Batch: N/A Instrument ID: BVMJ GC/MS Lab File ID: 1JB2730.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL MSD Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27893-21 Water 1.0 02/28/2009 0230 02/28/2009 0230 Analysis Batch: 660-75698 Prep Batch: N/A Instrument ID: BVMJ GC/MS Lab File ID: 1JB2731.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte MS Benzene Chlorobenzene 1,1-Dichloroethene Toluene Trichloroethene 108 105 102 105 107 % Rec. MSD 98 95 96 98 104 Limit RPD RPD Limit 62 - 135 72 - 127 46 - 147 68 - 131 56 - 143 10 10 6 8 3 37 22 30 33 35 MS Qual MSD Qual Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 185 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Method Blank - Batch: 660-75699 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-75699/2 Water 1.0 02/28/2009 0906 02/28/2009 0906 Method: 8260B Preparation: 5030B Analysis Batch: 660-75699 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JB2747.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 186 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Method Blank - Batch: 660-75699 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-75699/2 Water 1.0 02/28/2009 0906 02/28/2009 0906 Method: 8260B Preparation: 5030B Analysis Batch: 660-75699 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JB2747.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene 0.59 0.98 0.63 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 U U U U U U U U U U U U U U U U U U U U U U U U 0.59 0.98 0.63 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 1.0 2.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane % Rec Acceptance Limits 99 102 96 77 - 122 74 - 126 70 - 130 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 187 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Lab Control Spike - Batch: 660-75699 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: LCS 660-75699/1 Water 1.0 02/28/2009 0816 02/28/2009 0816 Method: 8260B Preparation: 5030B Analysis Batch: 660-75699 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JB2745.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Spike Amount Result % Rec. Limit Qual Benzene Chlorobenzene 1,1-Dichloroethene Toluene Trichloroethene 50.0 50.0 50.0 50.0 50.0 55.6 55.1 54.1 55.6 56.4 111 110 108 111 113 62 - 135 72 - 127 46 - 147 68 - 131 56 - 143 Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 660-75699 Method: 8260B Preparation: 5030B MS Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27893-26 Water 1.0 02/28/2009 1044 02/28/2009 1044 Analysis Batch: 660-75699 Prep Batch: N/A Instrument ID: BVMJ GC/MS Lab File ID: 1JB2751.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL MSD Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27893-26 Water 1.0 02/28/2009 1108 02/28/2009 1108 Analysis Batch: 660-75699 Prep Batch: N/A Instrument ID: BVMJ GC/MS Lab File ID: 1JB2752.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte MS Benzene Chlorobenzene 1,1-Dichloroethene Toluene Trichloroethene 100 97 97 100 101 % Rec. MSD 103 99 99 101 101 Limit RPD RPD Limit 62 - 135 72 - 127 46 - 147 68 - 131 56 - 143 3 2 2 1 0 37 22 30 33 35 MS Qual MSD Qual Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 188 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Method Blank - Batch: 660-75700 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-75700/2 Water 1.0 03/02/2009 1424 03/02/2009 1424 Method: 8260B Preparation: 5030B Analysis Batch: 660-75700 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JC0211.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL Benzene Bromobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 0.50 0.58 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.44 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 189 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Method Blank - Batch: 660-75700 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-75700/2 Water 1.0 03/02/2009 1424 03/02/2009 1424 Method: 8260B Preparation: 5030B Analysis Batch: 660-75700 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JC0211.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene 0.59 0.98 0.63 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 U U U U U U U U U U U U U U U U U U U U U U U U 0.59 0.98 0.63 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 1.0 2.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane % Rec Acceptance Limits 102 106 100 77 - 122 74 - 126 70 - 130 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 190 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Lab Control Spike - Batch: 660-75700 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: LCS 660-75700/1 Water 1.0 03/02/2009 1247 03/02/2009 1247 Method: 8260B Preparation: 5030B Analysis Batch: 660-75700 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JC0207.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Spike Amount Result % Rec. Limit Qual Benzene Chlorobenzene 1,1-Dichloroethene Toluene Trichloroethene 50.0 50.0 50.0 50.0 50.0 52.6 50.1 52.8 51.1 55.9 105 100 106 102 112 62 - 135 72 - 127 46 - 147 68 - 131 56 - 143 Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 660-75700 Method: 8260B Preparation: 5030B MS Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27893-22 Water 1.0 03/02/2009 1602 03/02/2009 1602 Analysis Batch: 660-75700 Prep Batch: N/A Instrument ID: BVMJ GC/MS Lab File ID: 1JC0215.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL MSD Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27893-22 Water 1.0 03/02/2009 1626 03/02/2009 1626 Analysis Batch: 660-75700 Prep Batch: N/A Instrument ID: BVMJ GC/MS Lab File ID: 1JC0216.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte MS Benzene Chlorobenzene 1,1-Dichloroethene Toluene Trichloroethene 101 96 98 96 102 % Rec. MSD 105 99 101 100 104 Limit RPD RPD Limit 62 - 135 72 - 127 46 - 147 68 - 131 56 - 143 4 2 3 4 2 37 22 30 33 35 MS Qual MSD Qual Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 191 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Method Blank - Batch: 660-75525 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-75525/2 Water 1.0 02/27/2009 1200 02/27/2009 1200 Method: 8260C SIM/ID Preparation: 5030B Analysis Batch: 660-75525 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HB2713.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL 1,4-Dioxane 0.54 U 0.54 1.0 Lab Control Spike - Batch: 660-75525 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: LCS 660-75525/1 Water 1.0 02/27/2009 1052 02/27/2009 1052 Method: 8260C SIM/ID Preparation: 5030B Analysis Batch: 660-75525 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HB2709.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Spike Amount Result % Rec. Limit Qual 1,4-Dioxane 25.0 25.5 102 50 - 150 Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 660-75525 Method: 8260C SIM/ID Preparation: 5030B MS Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27890-C-3 MS Water 1.0 02/27/2009 1525 02/27/2009 1525 Analysis Batch: 660-75525 Prep Batch: N/A Instrument ID: BVMH GC/MS Lab File ID: 1HB2725.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL MSD Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27890-D-3 MSD Water 1.0 02/27/2009 1542 02/27/2009 1542 Analysis Batch: 660-75525 Prep Batch: N/A Instrument ID: BVMH GC/MS Lab File ID: 1HB2726.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte MS 1,4-Dioxane 100 % Rec. MSD 90 Limit RPD RPD Limit 50 - 150 11 50 MS Qual MSD Qual Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 192 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Method Blank - Batch: 660-75613 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-75613/2 Water 1.0 03/02/2009 1138 03/02/2009 1138 Method: 8260C SIM/ID Preparation: 5030B Analysis Batch: 660-75613 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HC0212.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL 1,4-Dioxane 0.54 U 0.54 1.0 Lab Control Spike - Batch: 660-75613 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: LCS 660-75613/1 Water 1.0 03/02/2009 1046 03/02/2009 1046 Method: 8260C SIM/ID Preparation: 5030B Analysis Batch: 660-75613 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HC0209.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Spike Amount Result % Rec. Limit Qual 1,4-Dioxane 25.0 27.3 109 50 - 150 Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 660-75613 Method: 8260C SIM/ID Preparation: 5030B MS Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27893-14 Water 1.0 03/02/2009 1756 03/02/2009 1756 Analysis Batch: 660-75613 Prep Batch: N/A Instrument ID: BVMH GC/MS Lab File ID: 1HC0234.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL MSD Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27893-14 Water 1.0 03/02/2009 1813 03/02/2009 1813 Analysis Batch: 660-75613 Prep Batch: N/A Instrument ID: BVMH GC/MS Lab File ID: 1HC0235.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte MS 1,4-Dioxane 102 % Rec. MSD 101 Limit RPD RPD Limit 50 - 150 0 50 MS Qual MSD Qual Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 193 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Method Blank - Batch: 660-75684 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-75684/3 Water 1.0 03/03/2009 1229 03/03/2009 1229 Method: 8260C SIM/ID Preparation: 5030B Analysis Batch: 660-75684 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HC0314.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL 1,4-Dioxane 0.54 U 0.54 1.0 Lab Control Spike - Batch: 660-75684 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: LCS 660-75684/1 Water 1.0 03/03/2009 1103 03/03/2009 1103 Method: 8260C SIM/ID Preparation: 5030B Analysis Batch: 660-75684 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HC0309.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Spike Amount Result % Rec. Limit 1,4-Dioxane 25.0 25.6 103 50 - 150 Matrix Spike - Batch: 660-75684 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27916-D-15 MS Water 1.0 03/03/2009 1429 03/03/2009 1429 Qual Method: 8260C SIM/ID Preparation: 5030B Analysis Batch: 660-75684 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HC0321.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Sample Result/Qual Spike Amount Result % Rec. 1,4-Dioxane 0.89 25.0 23.3 90 I Limit Qual 50 - 150 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 194 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Duplicate - Batch: 660-75684 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27916-B-13 DU Water 1.0 03/03/2009 1355 03/03/2009 1355 Method: 8260C SIM/ID Preparation: 5030B Analysis Batch: 660-75684 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HC0319.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Sample Result/Qual Result RPD Limit 1,4-Dioxane 13 17.2 28 50 Qual Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 195 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Method Blank - Batch: 660-75694 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-75694/2 Water 1.0 02/28/2009 0051 02/28/2009 0051 Method: 8260C SIM/ID Preparation: 5030B Analysis Batch: 660-75694 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JB2727.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL 1,4-Dioxane 0.54 U 0.54 1.0 Lab Control Spike - Batch: 660-75694 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: LCS 660-75694/1 Water 1.0 02/28/2009 0026 02/28/2009 0026 Method: 8260C SIM/ID Preparation: 5030B Analysis Batch: 660-75694 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JB2726.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Spike Amount Result % Rec. Limit Qual 1,4-Dioxane 25.0 25.1 100 50 - 150 Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 660-75694 Method: 8260C SIM/ID Preparation: 5030B MS Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27893-21 Water 1.0 02/28/2009 0205 02/28/2009 0205 Analysis Batch: 660-75694 Prep Batch: N/A Instrument ID: BVMJ GC/MS Lab File ID: 1JB2730.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL MSD Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27893-21 Water 1.0 02/28/2009 0230 02/28/2009 0230 Analysis Batch: 660-75694 Prep Batch: N/A Instrument ID: BVMJ GC/MS Lab File ID: 1JB2731.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte MS 1,4-Dioxane 115 % Rec. MSD 91 Limit RPD RPD Limit 50 - 150 24 50 MS Qual MSD Qual Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 196 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Method Blank - Batch: 660-75695 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-75695/2 Water 1.0 02/28/2009 0930 02/28/2009 0930 Method: 8260C SIM/ID Preparation: 5030B Analysis Batch: 660-75695 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JB2748.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL 1,4-Dioxane 0.54 U 0.54 1.0 Lab Control Spike - Batch: 660-75695 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: LCS 660-75695/1 Water 1.0 02/28/2009 0816 02/28/2009 0816 Method: 8260C SIM/ID Preparation: 5030B Analysis Batch: 660-75695 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JB2745.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Spike Amount Result % Rec. Limit Qual 1,4-Dioxane 25.0 30.5 122 50 - 150 Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 660-75695 Method: 8260C SIM/ID Preparation: 5030B MS Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27893-26 Water 1.0 02/28/2009 1044 02/28/2009 1044 Analysis Batch: 660-75695 Prep Batch: N/A Instrument ID: BVMJ GC/MS Lab File ID: 1JB2751.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL MSD Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27893-26 Water 1.0 02/28/2009 1108 02/28/2009 1108 Analysis Batch: 660-75695 Prep Batch: N/A Instrument ID: BVMJ GC/MS Lab File ID: 1JB2752.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte MS 1,4-Dioxane 104 % Rec. MSD 107 Limit RPD RPD Limit 50 - 150 1 50 MS Qual MSD Qual Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 197 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Method Blank - Batch: 660-75696 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-75696/1 Water 1.0 03/02/2009 1424 03/02/2009 1424 Method: 8260C SIM/ID Preparation: 5030B Analysis Batch: 660-75696 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JC0211.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL 1,4-Dioxane 0.54 U 0.54 1.0 Lab Control Spike - Batch: 660-75696 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: LCS 660-75696/2 Water 1.0 03/02/2009 1449 03/02/2009 1449 Method: 8260C SIM/ID Preparation: 5030B Analysis Batch: 660-75696 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JC0212.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Spike Amount Result % Rec. Limit Qual 1,4-Dioxane 25.0 18.6 74 50 - 150 Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 660-75696 Method: 8260C SIM/ID Preparation: 5030B MS Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27893-22 Water 1.0 03/02/2009 1602 03/02/2009 1602 Analysis Batch: 660-75696 Prep Batch: N/A Instrument ID: BVMJ GC/MS Lab File ID: 1JC0215.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL MSD Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27893-22 Water 1.0 03/02/2009 1626 03/02/2009 1626 Analysis Batch: 660-75696 Prep Batch: N/A Instrument ID: BVMJ GC/MS Lab File ID: 1JC0216.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte MS 1,4-Dioxane 94 % Rec. MSD 94 Limit RPD RPD Limit 50 - 150 0 50 MS Qual MSD Qual Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 198 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Method Blank - Batch: 660-75517 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-75517/1-A Water 1.0 03/03/2009 1254 02/27/2009 1027 Method: 6010B Preparation: 3005A Total Recoverable Analysis Batch: 660-75689 Prep Batch: 660-75517 Units: mg/L Instrument ID: TJA ICP TRACE Lab File ID: 9C03A Initial Weight/Volume: 50 mL Final Weight/Volume: 50 mL Analyte Result Qual MDL PQL Calcium Iron Iron, Dissolved Potassium Magnesium Manganese Manganese, Dissolved Sodium 0.10 0.050 0.050 0.19 0.020 0.0010 0.0010 0.31 U U U U U U U U 0.10 0.050 0.050 0.19 0.020 0.0010 0.0010 0.31 0.50 0.20 0.20 1.0 0.080 0.0040 0.0040 0.50 Lab Control Spike - Batch: 660-75517 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: LCS 660-75517/2-A Water 1.0 03/03/2009 1300 02/27/2009 1027 Method: 6010B Preparation: 3005A Total Recoverable Analysis Batch: 660-75689 Prep Batch: 660-75517 Units: mg/L Instrument ID: TJA ICP TRACE Lab File ID: 9C03A Initial Weight/Volume: 50 mL Final Weight/Volume: 50 mL Analyte Spike Amount Result % Rec. Limit Calcium Iron Iron, Dissolved Potassium Magnesium Manganese Manganese, Dissolved Sodium 1.00 1.00 1.00 10.0 1.00 1.00 1.00 10.0 0.962 0.969 0.969 8.81 0.929 0.966 0.966 9.71 96 97 97 88 93 97 97 97 75 - 125 75 - 125 75 - 125 75 - 125 75 - 125 75 - 125 75 - 125 75 - 125 Qual Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 199 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 660-75517 Method: 6010B Preparation: 3005A Total Recoverable MS Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27893-41 Water 1.0 03/03/2009 1330 02/27/2009 1027 Analysis Batch: 660-75689 Prep Batch: 660-75517 Instrument ID: TJA ICP TRACE Lab File ID: 9C03A Initial Weight/Volume: 50 mL Final Weight/Volume: 50 mL MSD Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27893-41 Water 1.0 03/03/2009 1335 02/27/2009 1027 Analysis Batch: 660-75689 Prep Batch: 660-75517 Instrument ID: TJA ICP TRACE Lab File ID: 9C03A Initial Weight/Volume: 50 mL Final Weight/Volume: 50 mL Analyte MS Calcium Iron Iron, Dissolved Potassium Magnesium Manganese Manganese, Dissolved Sodium 430 138 138 104 107 97 97 124 % Rec. MSD 57 106 106 101 95 96 96 109 Limit RPD RPD Limit MS Qual MSD Qual 75 - 125 75 - 125 75 - 125 75 - 125 75 - 125 75 - 125 75 - 125 75 - 125 3 3 3 3 3 1 1 3 20 20 20 20 20 20 20 20 J3 J3 J3 J3 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 200 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Method Blank - Batch: 660-75752 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-75752/3 Water 1.0 03/02/2009 1717 N/A Method: 300.0 Preparation: N/A Analysis Batch: 660-75752 Prep Batch: N/A Units: mg/L Instrument ID: ICS 2000 Lab File ID: N/A Initial Weight/Volume: Final Weight/Volume: 2 mL Analyte Result Qual MDL PQL Bromide Chloride 0.027 0.20 U U 0.027 0.20 0.050 0.50 Method Blank - Batch: 660-75752 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-75752/19 Water 1.0 03/03/2009 1416 N/A Method: 300.0 Preparation: N/A Analysis Batch: 660-75752 Prep Batch: N/A Units: mg/L Instrument ID: ICS 2000 Lab File ID: N/A Initial Weight/Volume: Final Weight/Volume: 2 mL Analyte Result Qual MDL PQL Sulfate 0.20 U 0.20 0.50 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 201 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Lab Control Spike - Batch: 660-75752 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: LCS 660-75752/4 Water 1.0 03/02/2009 1743 N/A Method: 300.0 Preparation: N/A Analysis Batch: 660-75752 Prep Batch: N/A Units: mg/L Instrument ID: ICS 2000 Lab File ID: N/A Initial Weight/Volume: Final Weight/Volume: 2 mL Analyte Spike Amount Result % Rec. Limit Bromide Chloride 1.00 10.0 0.994 10.1 99 101 90 - 110 90 - 110 Lab Control Spike - Batch: 660-75752 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: LCS 660-75752/20 Water 1.0 03/03/2009 1442 N/A Qual Method: 300.0 Preparation: N/A Analysis Batch: 660-75752 Prep Batch: N/A Units: mg/L Instrument ID: ICS 2000 Lab File ID: N/A Initial Weight/Volume: Final Weight/Volume: 2 mL Analyte Spike Amount Result % Rec. Limit Sulfate 10.0 10.2 102 90 - 110 Qual Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 202 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 660-75752 Method: 300.0 Preparation: N/A MS Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27893-41 Water 2.0 03/02/2009 1835 N/A Analysis Batch: 660-75752 Prep Batch: N/A Instrument ID: ICS 2000 Lab File ID: N/A Initial Weight/Volume: Final Weight/Volume: 2 mL MSD Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27893-41 Water 2.0 03/02/2009 1900 N/A Analysis Batch: 660-75752 Prep Batch: N/A Instrument ID: ICS 2000 Lab File ID: N/A Initial Weight/Volume: Final Weight/Volume: 2 mL Analyte MS Bromide 100 % Rec. MSD 102 Limit RPD RPD Limit 90 - 110 1 30 MS Qual MSD Qual Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 660-75752 Method: 300.0 Preparation: N/A MS Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27893-41 Water 2.0 03/04/2009 1450 N/A Analysis Batch: 660-75752 Prep Batch: N/A Instrument ID: ICS 2000 Lab File ID: N/A Initial Weight/Volume: Final Weight/Volume: 5 mL MSD Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27893-41 Water 2.0 03/04/2009 1502 N/A Analysis Batch: 660-75752 Prep Batch: N/A Instrument ID: ICS 2000 Lab File ID: N/A Initial Weight/Volume: Final Weight/Volume: 5 mL Analyte MS Chloride Sulfate 656 178 % Rec. MSD 664 179 Limit RPD RPD Limit MS Qual MSD Qual 90 - 110 90 - 110 0 0 30 30 J3 J3 J3 J3 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 203 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Method Blank - Batch: 660-75441 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-75441/1 Water 1.0 02/26/2009 0841 N/A Method: 353.2 Preparation: N/A Analysis Batch: 660-75441 Prep Batch: N/A Units: mg/L Instrument ID: No Equipment Assigned Lab File ID: N/A Initial Weight/Volume: 50 mL Final Weight/Volume: 50 mL Analyte Result Qual MDL PQL Nitrite as N Nitrate as N 0.10 0.10 U U 0.10 0.10 0.50 0.50 Lab Control Spike - Batch: 660-75441 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: LCS 660-75441/2 Water 1.0 02/26/2009 0841 N/A Method: 353.2 Preparation: N/A Analysis Batch: 660-75441 Prep Batch: N/A Units: mg/L Instrument ID: No Equipment Assigned Lab File ID: N/A Initial Weight/Volume: 100 mL Final Weight/Volume: 100 mL Analyte Spike Amount Result % Rec. Limit Nitrite as N 1.00 0.923 92 90 - 110 Qual Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 204 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 660-75441 Method: 353.2 Preparation: N/A MS Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27852-Z-1 MS Water 1.0 02/26/2009 0841 N/A Analysis Batch: 660-75441 Prep Batch: N/A Instrument ID: No Equipment Assigned Lab File ID: N/A Initial Weight/Volume: 50 mL Final Weight/Volume: 50 mL MSD Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27852-Z-1 MSD Water 1.0 02/26/2009 0841 N/A Analysis Batch: 660-75441 Prep Batch: N/A Instrument ID: No Equipment Assigned Lab File ID: N/A Initial Weight/Volume: 50 mL Final Weight/Volume: 50 mL Analyte MS Nitrite as N 110 % Rec. MSD 97 Limit RPD RPD Limit 90 - 110 12 30 MS Qual MSD Qual Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 205 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Method Blank - Batch: 660-75644 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-75644/1 Water 1.0 03/02/2009 1303 03/02/2009 1303 Method: 353.2 Preparation: 353.2 Analysis Batch: 660-75644 Prep Batch: N/A Units: mg/L Instrument ID: No Equipment Assigned Lab File ID: N/A Initial Weight/Volume: 50 mL Final Weight/Volume: 50 mL Analyte Result Qual MDL PQL Nitrate Nitrite as N 0.10 U 0.10 0.50 Lab Control Spike - Batch: 660-75644 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: LCS 660-75644/2 Water 1.0 03/02/2009 1303 03/02/2009 1303 Method: 353.2 Preparation: 353.2 Analysis Batch: 660-75644 Prep Batch: N/A Units: mg/L Instrument ID: No Equipment Assigned Lab File ID: N/A Initial Weight/Volume: 100 mL Final Weight/Volume: 100 mL Analyte Spike Amount Result % Rec. Limit Qual Nitrate Nitrite as N 1.00 0.972 97 90 - 110 Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 660-75644 Method: 353.2 Preparation: 353.2 MS Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27893-48 Water 1.0 03/02/2009 1303 03/02/2009 1303 Analysis Batch: 660-75644 Prep Batch: N/A Instrument ID: No Equipment Assigned Lab File ID: N/A Initial Weight/Volume: 50 mL Final Weight/Volume: 50 mL MSD Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27893-48 Water 1.0 03/02/2009 1303 03/02/2009 1303 Analysis Batch: 660-75644 Prep Batch: N/A Instrument ID: No Equipment Assigned Lab File ID: N/A Initial Weight/Volume: 50 mL Final Weight/Volume: 50 mL Analyte MS Nitrate Nitrite as N 96 % Rec. MSD 88 Limit RPD RPD Limit 90 - 110 8 30 MS Qual MSD Qual J3 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 206 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Method Blank - Batch: 660-75553 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-75553/3 Water 1.0 02/27/2009 1037 N/A Method: SM 2320B Preparation: N/A Analysis Batch: 660-75553 Prep Batch: N/A Units: mg/L Instrument ID: Titrator Instrument Lab File ID: N/A Initial Weight/Volume: 50 mL Final Weight/Volume: 50 mL Analyte Result Qual PQL PQL Alkalinity Bicarbonate Alkalinity as CaCO3 Carbonate Alkalinity as CaCO3 Hydroxide Alkalinity Phenolphthalein Alkalinity 1.0 1.0 1.0 1.0 1.0 U U U U U 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 Lab Control Spike - Batch: 660-75553 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: LCS 660-75553/4 Water 1.0 02/27/2009 1045 N/A Method: SM 2320B Preparation: N/A Analysis Batch: 660-75553 Prep Batch: N/A Units: mg/L Instrument ID: Titrator Instrument Lab File ID: N/A Initial Weight/Volume: 50 mL Final Weight/Volume: 50 mL Analyte Spike Amount Result % Rec. Limit Alkalinity 118 124 105 80 - 120 Duplicate - Batch: 660-75553 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27893-46 Water 1.0 02/27/2009 1322 N/A Qual Method: SM 2320B Preparation: N/A Analysis Batch: 660-75553 Prep Batch: N/A Units: mg/L Instrument ID: Titrator Instrument Lab File ID: N/A Initial Weight/Volume: 50 mL Final Weight/Volume: 50 mL Analyte Sample Result/Qual Result RPD Alkalinity Bicarbonate Alkalinity as CaCO3 Carbonate Alkalinity as CaCO3 Hydroxide Alkalinity Phenolphthalein Alkalinity 130 130 1.0 1.0 1.0 138 138 1.0 1.0 1.0 2.36 2.36 NC NC NC U U U Limit Qual U U U Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 207 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Method Blank - Batch: 660-75622 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-75622/3 Water 1.0 03/02/2009 0907 N/A Method: SM 2320B Preparation: N/A Analysis Batch: 660-75622 Prep Batch: N/A Units: mg/L Instrument ID: Titrator Instrument Lab File ID: N/A Initial Weight/Volume: 50 mL Final Weight/Volume: 50 mL Analyte Result Qual PQL PQL Alkalinity Bicarbonate Alkalinity as CaCO3 Carbonate Alkalinity as CaCO3 Hydroxide Alkalinity Phenolphthalein Alkalinity 1.0 1.0 1.0 1.0 1.0 U U U U U 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 Lab Control Spike - Batch: 660-75622 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: LCS 660-75622/4 Water 1.0 03/02/2009 0915 N/A Method: SM 2320B Preparation: N/A Analysis Batch: 660-75622 Prep Batch: N/A Units: mg/L Instrument ID: Titrator Instrument Lab File ID: N/A Initial Weight/Volume: 50 mL Final Weight/Volume: 50 mL Analyte Spike Amount Result % Rec. Limit Alkalinity 118 127 108 80 - 120 Duplicate - Batch: 660-75622 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27893-47 Water 1.0 03/02/2009 0925 N/A Qual Method: SM 2320B Preparation: N/A Analysis Batch: 660-75622 Prep Batch: N/A Units: mg/L Instrument ID: Titrator Instrument Lab File ID: N/A Initial Weight/Volume: 50 mL Final Weight/Volume: 50 mL Analyte Sample Result/Qual Result RPD Alkalinity Bicarbonate Alkalinity as CaCO3 Carbonate Alkalinity as CaCO3 Hydroxide Alkalinity Phenolphthalein Alkalinity 61 61 1.0 1.0 1.0 60.5 60.5 1.0 1.0 1.0 0.0330 0.0330 NC NC NC U U U Limit Qual U U U Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 208 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Method Blank - Batch: 640-54348 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 640-54348/1 Water 1.0 02/27/2009 1212 N/A Method: SM 2540C Preparation: N/A Analysis Batch: 640-54348 Prep Batch: N/A Units: mg/L Instrument ID: No Equipment Assigned Lab File ID: N/A Initial Weight/Volume: 200 mL Final Weight/Volume: 200 mL Analyte Result Qual MDL PQL Total Dissolved Solids 5.0 U 5.0 5.0 Lab Control Spike/ Lab Control Spike Duplicate Recovery Report - Batch: 640-54348 Method: SM 2540C Preparation: N/A LCS Lab Sample ID: LCS 640-54348/2 Client Matrix: Water Dilution: 1.0 02/27/2009 1212 Date Analyzed: Date Prepared: N/A Analysis Batch: 640-54348 Prep Batch: N/A Units: mg/L Instrument ID: No Equipment Assigned Lab File ID: N/A Initial Weight/Volume: 100 mL Final Weight/Volume: 200 mL LCSD Lab Sample ID: LCSD 640-54348/3 Client Matrix: Water Dilution: 1.0 02/27/2009 1212 Date Analyzed: Date Prepared: N/A Analysis Batch: 640-54348 Prep Batch: N/A Units: mg/L Instrument ID: No Equipment Assigned Lab File ID: N/A Initial Weight/Volume: 100 mL Final Weight/Volume: 200 mL Analyte LCS Total Dissolved Solids 98 % Rec. LCSD 102 Limit RPD RPD Limit 80 - 120 4 25 LCS Qual LCSD Qual Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 209 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Duplicate - Batch: 640-54348 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27893-41 Water 1.0 02/27/2009 1212 N/A Method: SM 2540C Preparation: N/A Analysis Batch: 640-54348 Prep Batch: N/A Units: mg/L Instrument ID: No Equipment Assigned Lab File ID: N/A Initial Weight/Volume: 100 mL Final Weight/Volume: 200 mL Analyte Sample Result/Qual Result RPD Limit Total Dissolved Solids 580 592 2 25 Qual Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 210 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Method Blank - Batch: 640-54352 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 640-54352/1 Water 1.0 02/27/2009 1228 N/A Method: SM 2540D Preparation: N/A Analysis Batch: 640-54352 Prep Batch: N/A Units: mg/L Instrument ID: No Equipment Assigned Lab File ID: N/A Initial Weight/Volume: 1000 mL Final Weight/Volume: 200 mL Analyte Result Qual MDL PQL Total Suspended Solids 0.48 U 0.48 1.0 Lab Control Spike/ Lab Control Spike Duplicate Recovery Report - Batch: 640-54352 Method: SM 2540D Preparation: N/A LCS Lab Sample ID: LCS 640-54352/2 Client Matrix: Water Dilution: 1.0 02/27/2009 1228 Date Analyzed: Date Prepared: N/A Analysis Batch: 640-54352 Prep Batch: N/A Units: mg/L Instrument ID: No Equipment Assigned Lab File ID: N/A Initial Weight/Volume: 200 mL Final Weight/Volume: 200 mL LCSD Lab Sample ID: LCSD 640-54352/3 Client Matrix: Water Dilution: 1.0 02/27/2009 1228 Date Analyzed: Date Prepared: N/A Analysis Batch: 640-54352 Prep Batch: N/A Units: mg/L Instrument ID: No Equipment Assigned Lab File ID: N/A Initial Weight/Volume: 200 mL Final Weight/Volume: 200 mL Analyte LCS Total Suspended Solids 90 % Rec. LCSD 90 Limit RPD RPD Limit 80 - 120 0 25 LCS Qual LCSD Qual Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 211 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Duplicate - Batch: 640-54352 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27893-41 Water 1.0 02/27/2009 1228 N/A Method: SM 2540D Preparation: N/A Analysis Batch: 640-54352 Prep Batch: N/A Units: mg/L Instrument ID: No Equipment Assigned Lab File ID: N/A Initial Weight/Volume: 200 mL Final Weight/Volume: 200 mL Analyte Sample Result/Qual Result RPD Limit Total Suspended Solids 65 58.5 11 25 Qual Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 212 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Method Blank - Batch: 660-75561 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-75561/1-A Water 1.0 02/27/2009 1500 02/27/2009 1220 Method: SM 5220D Preparation: SM 5220 Analysis Batch: 660-75563 Prep Batch: 660-75561 Units: mg/L Instrument ID: No Equipment Assigned Lab File ID: N/A Initial Weight/Volume: 2 mL Final Weight/Volume: 2 mL Analyte Result Qual MDL PQL Chemical Oxygen Demand 10 U 10 20 Lab Control Spike - Batch: 660-75561 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: LCS 660-75561/2-A Water 1.0 02/27/2009 1500 02/27/2009 1220 Method: SM 5220D Preparation: SM 5220 Analysis Batch: 660-75563 Prep Batch: 660-75561 Units: mg/L Instrument ID: No Equipment Assigned Lab File ID: N/A Initial Weight/Volume: 2 mL Final Weight/Volume: 2 mL Analyte Spike Amount Result % Rec. Limit Qual Chemical Oxygen Demand 50.0 52.2 104 90 - 110 Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 660-75561 Method: SM 5220D Preparation: SM 5220 MS Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27893-45 Water 1.0 02/27/2009 1500 02/27/2009 1220 Analysis Batch: 660-75563 Prep Batch: 660-75561 Instrument ID: No Equipment Assigned Lab File ID: N/A Initial Weight/Volume: 2 mL Final Weight/Volume: 2 mL MSD Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27893-45 Water 1.0 02/27/2009 1500 02/27/2009 1220 Analysis Batch: 660-75563 Prep Batch: 660-75561 Instrument ID: No Equipment Assigned Lab File ID: N/A Initial Weight/Volume: 2 mL Final Weight/Volume: 2 mL Analyte MS Chemical Oxygen Demand 94 % Rec. MSD 92 Limit RPD RPD Limit 90 - 110 2 20 MS Qual MSD Qual Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 213 of 221 04/06/2009 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Method Blank - Batch: 660-75675 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-75675/5 Water 1.0 03/02/2009 1936 N/A Method: SM 5310C Preparation: N/A Analysis Batch: 660-75675 Prep Batch: N/A Units: mg/L Instrument ID: Teledyne TOC Analyzer Lab File ID: 03021812 Initial Weight/Volume: Final Weight/Volume: 40 mL Analyte Result Qual MDL PQL Total Organic Carbon 0.53 U 0.53 1.0 Lab Control Spike - Batch: 660-75675 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: LCS 660-75675/6 Water 1.0 03/02/2009 1958 N/A Method: SM 5310C Preparation: N/A Analysis Batch: 660-75675 Prep Batch: N/A Units: mg/L Instrument ID: Teledyne TOC Analyzer Lab File ID: 03021812 Initial Weight/Volume: Final Weight/Volume: 40 mL Analyte Spike Amount Result % Rec. Limit Qual Total Organic Carbon 10.0 9.08 91 80 - 120 Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 660-75675 Method: SM 5310C Preparation: N/A MS Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27893-43 Water 1.0 03/02/2009 2141 N/A Analysis Batch: 660-75675 Prep Batch: N/A Instrument ID: Teledyne TOC Analyzer Lab File ID: 03021812 Initial Weight/Volume: Final Weight/Volume: 40 mL MSD Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-27893-43 Water 1.0 03/02/2009 2208 N/A Analysis Batch: 660-75675 Prep Batch: N/A Instrument ID: Teledyne TOC Analyzer Lab File ID: 03021812 Initial Weight/Volume: Final Weight/Volume: 40 mL Analyte MS Total Organic Carbon 91 % Rec. MSD 90 Limit RPD RPD Limit 80 - 120 0 25 MS Qual MSD Qual Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 214 of 221 04/06/2009 Page 215 of 221 04/06/2009 Page 216 of 221 04/06/2009 Page 217 of 221 04/06/2009 Page 218 of 221 04/06/2009 Page 219 of 221 04/06/2009 Login Sample Receipt Check List Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Login Number: 27893 Creator: Harrison, Amanda List Number: 1 List Source: TestAmerica Tampa Question T / F/ NA Radioactivity either was not measured or, if measured, is at or below background The cooler's custody seal, if present, is intact. N/A The cooler or samples do not appear to have been compromised or tampered with. Samples were received on ice. Cooler Temperature is acceptable. True Cooler Temperature is recorded. COC is present. COC is filled out in ink and legible. COC is filled out with all pertinent information. There are no discrepancies between the sample IDs on the containers and the COC. Samples are received within Holding Time. Sample containers have legible labels. Containers are not broken or leaking. True True True True True Sample collection date/times are provided. Appropriate sample containers are used. Sample bottles are completely filled. There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs VOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter. If necessary, staff have been informed of any short hold time or quick TAT needs Multiphasic samples are not present. Samples do not require splitting or compositing. True True True True TestAmerica Tampa Comment N/A True True 2.9, 3.6, 3.1, and 4.0 degrees C CU-07 True True True True True True True Page 220 of 221 04/06/2009 Login Sample Receipt Check List Client: ARCADIS U.S., Inc. Job Number: 660-27893-1 Login Number: 27893 Creator: Jones, Daniella List Number: 1 List Source: TestAmerica Tallahassee List Creation: 02/27/09 08:04 AM Question T / F/ NA Radioactivity either was not measured or, if measured, is at or below background The cooler's custody seal, if present, is intact. N/A The cooler or samples do not appear to have been compromised or tampered with. Samples were received on ice. Cooler Temperature is acceptable. True Cooler Temperature is recorded. COC is present. COC is filled out in ink and legible. COC is filled out with all pertinent information. There are no discrepancies between the sample IDs on the containers and the COC. Samples are received within Holding Time. Sample containers have legible labels. Containers are not broken or leaking. True True True True True Sample collection date/times are provided. Appropriate sample containers are used. Sample bottles are completely filled. There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs VOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter. If necessary, staff have been informed of any short hold time or quick TAT needs Multiphasic samples are not present. Samples do not require splitting or compositing. True True True True TestAmerica Tampa Comment True True True True True True N/A True True True Page 221 of 221 04/06/2009 MONITOR WELL CONSTRUCTION SCHEMATIC DIAGRAM Client Raytheon Site Location St. Petersburg Fl Well Location Median of 68th St N, 490 ft south of 68th St N & Crosswind Dr, St. Petersburg FL Project No. TF00922.0043 Contractor PDS Driller(s) Jon, Sergio, Eucoio Drilling Method(s) Direct Push Prepared By M. Sedor Date(s) Installed 11/13/2009 Monitor Well No. DMW-CC Survey Datum Ground Elevation Type of Protective Cover 8" Manhole Type of Riser Pipe 1" Sch 40 PVC Diameter of Borehole 1.5 inches Type of Grout Around Riser Pipe Portland Type I/II Cement Grout Depth Top of Seal 44 feet Type of Seal Prepacked bentonite Depth Bottom of Seal 47 feet Depth Top of Screen under 30/65 silica sand 47 feet Screen Section Material Screen Size 1" Sch 40 PVC 0.01 Type of Sand Pack Around Screen 20/30 silica prepacked sand Depth Bottom of Screen 47 feet Depth Bottom of Borehole/Sandpack 50 feet REMARKS: PROJ\FORMS\FIELD\DMW-CC Construction.xlsx Florida Department of Environmental Protection - Division of Waste Management - Bureau of Petroleum Storage Systems WELL CONSTRUCTION AND DEVELOPMENT LOG WELL CONSTRUCTION DATA Site Name: Well Number: DMW-CC Well Location and Type (check appropriate boxes): On-Site FDEP Facility I.D. Number: RAYTHEON Well Purpose: Right-of-Way Perched Monitoring Shallow (Water-T able ) Monitoring Flush-to-Grade Intermediate or Deep Monit Monitoring oring Remediation or Other (describe) Off-Site Private Property Above Grade (AG) Well Install Date(s): 11/13/09 Well Install Method: Direct Push Surface Casing Install Method: N/A If AG, list feet of riser above land surface: Well Depth Borehole Depth 55 (feet): Borehole Diameter Manhole Diameter 52 (feet): (inches): 2.5 Riser/Screen Connections: Riser Diameter and Material: 1" Schedule 40 PVC Screen Diameter and Material: Permanent 2 Surface Casing Material: Permanent Permanent N/A 3 Surface Casing Material: Permanent Permanent 3 Surface Casing I.D. (inches): Yes Filter Pack Seal Material and Size: 0 from Surface Seal Material: / C Portland type I/II Cement G Grout feet to 5 52 feet to 3 Filter Pack Seal Length: from 47 feet to 44 Surface Seal Length: from feet feet Filter Pack Length: No 2' prepacked bentonite packer below 1' of 30/65 Silica Sand feet to 3 Surface Casing Length: from Filter Pack Material and Size: Prepacked Filter Around Screen (check one): 20/30 Silica Sand 0 feet feet rd T emporary feet 47 feet feet to 2 Surface Casing Length: from rd 0 feet nd T emporary rd also check: 2 Surface Casing I.D. (inches): N/A feet to 0 from nd feet feet 52 1st Surface Casing Length: T emporary nd also check: 1st Surface Casing I.D. (inches): N/A feet to 5 from 2 feet 47 Screen Length: 0.01 by 47 from Other (describe) Screen Slot Size: 1st Surface Casing Material: feet Riser Length: Flush-T hreaded 1" Schedule 40 PVC also check: 8 (inches): Well Pad Size: 2 44 feet to feet feet 47 feet feet 44 feet feet 0 feet WELL DEVELOPMENT DATA Well Development Date: Well Development Method (check one): Development Pump Type (check): Submersible Centrifugal Peristaltic Pump Compressed Air Depth to Groundwater (before developing in feet): Other (describe) Pumping Rate (gallons per minute): ~0.7 Pumping Condition (check one): Continuous Surge/Pump Other (describe) 11/16/09 Intermittent Maximum Drawdown of Groundwater During Development (feet): N/A Total Development Water Removed (gallons): Water Appearance (color and odor) At Start of Development: Brown 25 3.70 Well Purged Dry (check one): Yes No Development Duration Development Water Drummed (check one): (minutes): Yes 35 Water Appearance (color and odor) At End of Development: Clear WELL CONSTRUCTION OR DEVELOPMENT REMARKS No MONITOR WELL CONSTRUCTION SCHEMATIC DIAGRAM Client Raytheon Site Location St. Petersburg Fl Well Location Median of 68th St N, 490 ft south of 68th St N & Crosswind Dr, St. Petersburg FL Project No. TF00922.0043 Contractor PDS Driller(s) Jon, Sergio, Eucoio Drilling Method(s) Direct Push Prepared By M. Sedor Date(s) Installed 11/13/2009 Monitor Well No. IMW-V Survey Datum Ground Elevation Type of Protective Cover 8" Manhole Type of Riser Pipe 1" Sch 40 PVC Diameter of Borehole 1.5 inches Type of Grout Around Riser Pipe Portland Type I/II Cement Grout Depth Top of Seal 31 feet Type of Seal 30/65 silica sand Depth Bottom of Seal 33 feet Depth Top of Screen 34 feet Screen Section Material Screen Size 1" Sch 40 PVC 0.01 Type of Sand Pack Around Screen 20/30 silica prepacked sand+poured sand Depth Bottom of Screen 39 feet Depth Bottom of Borehole/Sandpack 39 feet REMARKS: PROJ\FORMS\FIELD\IMW-V Construction.xlsx Florida Department of Environmental Protection - Division of Waste Management - Bureau of Petroleum Storage Systems WELL CONSTRUCTION AND DEVELOPMENT LOG WELL CONSTRUCTION DATA Site Name: Well Number: IMW-V Well Location and Type (check appropriate boxes): On-Site FDEP Facility I.D. Number: RAYTHEON Well Purpose: Right-of-Way Perched Monitoring Shallow (Water-T able ) Monitoring Flush-to-Grade Intermediate or Deep Monit Monitoring oring Remediation or Other (describe) Off-Site Private Property Above Grade (AG) Well Install Date(s): 11/13/09 Well Install Method: Direct Push Surface Casing Install Method: N/A If AG, list feet of riser above land surface: Well Depth Borehole Depth 39 (feet): Borehole Diameter Manhole Diameter 39 (feet): (inches): 2.5 Riser/Screen Connections: Riser Diameter and Material: 1" Schedule 40 PVC Screen Diameter and Material: Permanent 2 Surface Casing Material: Permanent Permanent N/A 3 Surface Casing Material: Permanent Permanent 3 Surface Casing I.D. (inches): Yes Filter Pack Seal Material and Size: feet to 0 feet to 6 Filter Pack Length: No from 39 feet to 2 Filter Pack Seal Length: 30/65 Silica Sand from Surface Seal Material: / C Portland type I/II Cement G Grout 33 feet to 44 Surface Seal Length: from feet feet 3 Surface Casing Length: from Filter Pack Material and Size: Prepacked Filter Around Screen (check one): 20/30 Silica Sand 0 feet feet rd T emporary feet 34 feet feet to 2 Surface Casing Length: from rd 0 feet nd T emporary rd also check: 2 Surface Casing I.D. (inches): N/A feet to 0 from nd feet feet 39 1st Surface Casing Length: T emporary nd also check: 1st Surface Casing I.D. (inches): N/A feet to 5 from 2 feet 34 Screen Length: 0.01 by 34 from Other (describe) Screen Slot Size: 1st Surface Casing Material: feet Riser Length: Flush-T hreaded 1" Schedule 40 PVC also check: 8 (inches): Well Pad Size: 2 31 feet to feet feet 33 feet feet 31 feet feet 0 feet WELL DEVELOPMENT DATA Well Development Date: Well Development Method (check one): Development Pump Type (check): Submersible Centrifugal Peristaltic Pump Compressed Air Depth to Groundwater (before developing in feet): Other (describe) Pumping Rate (gallons per minute): ~0.7 Pumping Condition (check one): Continuous Surge/Pump Other (describe) 11/16/09 Intermittent Maximum Drawdown of Groundwater During Development (feet): N/A Total Development Water Removed (gallons): Water Appearance (color and odor) At Start of Development: Brown 20 4.35 Well Purged Dry (check one): Yes No Development Duration Development Water Drummed (check one): (minutes): Yes 30 Water Appearance (color and odor) At End of Development: Clear WELL CONSTRUCTION OR DEVELOPMENT REMARKS Note that the prepacked filter was 5 feet, but was surrounded by 6 feet of poured filter pack below the seal No ANALYTICAL REPORT Job Number: 660-32642-1 Job Description: Raytheon For: ARCADIS U.S., Inc. 14055 Riveredge Drive Suite 400 Tampa, FL 33637 Attention: Mr. Gus Suarez _____________________________________________ Approved for release. Natalie Tafuni Project Manager I 11/30/2009 3:31 PM Natalie Tafuni Project Manager I [email protected] 11/30/2009 cc: Ms. Lyndi Mott Mr. Melvin Rivera Albert Zumbuhl Methods: FDEP, DOH Certification #: TestAmerica Tampa E84282 These test results meet all the requirements of NELAC unless specified in the case narrative. All questions regarding this test report should be directed to the TestAmerica Project Manager who signed this test report. The estimated uncertainty associated with these reported results is available upon request. The results contained in this test report relate only to these samples included herein. TestAmerica Laboratories, Inc. TestAmerica Tampa 6712 Benjamin Road, Suite 100, Tampa, FL 33634 Tel (813) 885-7427 Fax (813) 885-7049 www.testamericainc.com Page 1 of 31 Job Narrative 660-32642-1 Comments No additional comments. Receipt All samples were received in good condition within temperature requirements. 8260B The laboratory control sample (LCS) for batch 660-87646 was outside of control limits for MIBK and 2-hexanone. These compounds are biased high in the LCS and the samples are non detect for MIBK and 2-hexanone. The data are flagged with J3 qualifiers. The batch matrix spike (MS) for batch 660-87646(job 660-32564) was outside of control limits for cis-1,3 dichloropropene, MIBK and 2-hexanone. The laboratory control sample (LCS) was withinn control criteria except as noted above. The data are flagged with J3 qualifiers. The sample duplicate %RPD for batch 660-87646 has a result of NC for most compounds. The sample result and the sample duplicate result are both Non-detect for these compounds. The Laboratory LIMs system flags the %RPD in this scenario as NC, or "not calculated". 8260C The batch matrix spike (MS) for batch 660-87653(job 660-32643) was over calibration range for 1,4-dioxane. The data are flagged with L qualifiers. Page 2 of 31 EXECUTIVE SUMMARY - Detections Client: ARCADIS U.S., Inc. Lab Sample ID Analyte 660-32642-1 Carbon disulfide 1,4-Dioxane Job Number: 660-32642-1 Client Sample ID Result / Qualifier Reporting Limit Units Method ug/L ug/L 8260B 8260C _SIM/ID IMW-V_111909 0.93 5.7 I TestAmerica Tampa Page 3 of 31 1.0 2.0 METHOD SUMMARY Client: ARCADIS U.S., Inc. Description Job Number: 660-32642-1 Lab Location Method Preparation Method Volatile Organic Compounds (GC/MS) Purge and Trap TAL TAM TAL TAM SW846 8260B SW846 5030B 1,4-Dioxane by SIM/Isotopic Dilution Purge and Trap TAL TAM TAL TAM SW846 8260C _SIM/ID SW846 5030C Matrix Water Lab References: TAL TAM = TestAmerica Tampa Method References: SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. TestAmerica Tampa Page 4 of 31 METHOD / ANALYST SUMMARY Client: ARCADIS U.S., Inc. Job Number: 660-32642-1 Method Analyst SW846 8260B Perrin, Todd TP SW846 8260C _SIM/ID Perrin, Todd TP TestAmerica Tampa Page 5 of 31 Analyst ID SAMPLE SUMMARY Client: ARCADIS U.S., Inc. Job Number: 660-32642-1 Lab Sample ID Client Sample ID Client Matrix 660-32642-1 660-32642-2 660-32642-3 IMW-V_111909 DMW-CC_111909 Trip Blank#4_111909 Water Water Water TestAmerica Tampa Page 6 of 31 Date/Time Sampled Date/Time Received 11/19/2009 1638 11/19/2009 1715 11/19/2009 0000 11/20/2009 1045 11/20/2009 1045 11/20/2009 1045 SAMPLE RESULTS TestAmerica Tampa Page 7 of 31 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IMW-V_111909 Lab Sample ID: Client Matrix: 660-32642-1 Water Job Number: 660-32642-1 Date Sampled: 11/19/2009 1638 Date Received: 11/20/2009 1045 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 11/20/2009 1832 11/20/2009 1832 Analyte Benzene Bromobenzene 1,2-Dichlorobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene TestAmerica Tampa Analysis Batch: 660-87646 Result (ug/L) 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 0.15 0.50 Page 8 of 31 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 0.15 0.50 BVMH5973 1HK2024.D 5 mL 5 mL PQL 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 1.0 1.0 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IMW-V_111909 Lab Sample ID: Client Matrix: 660-32642-1 Water Job Number: 660-32642-1 Date Sampled: 11/19/2009 1638 Date Received: 11/20/2009 1045 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 11/20/2009 1832 11/20/2009 1832 Analysis Batch: 660-87646 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Analyte Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Result (ug/L) 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.93 4.4 0.44 0.60 Qualifier U U U U U U U U U U U U U U U J3 I U J3 U U Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane %Rec 111 95 93 Qualifier TestAmerica Tampa Page 9 of 31 MDL 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 BVMH5973 1HK2024.D 5 mL 5 mL PQL 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 70 - 130 70 - 130 70 - 130 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-CC_111909 Lab Sample ID: Client Matrix: 660-32642-2 Water Job Number: 660-32642-1 Date Sampled: 11/19/2009 1715 Date Received: 11/20/2009 1045 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 11/20/2009 1917 11/20/2009 1917 Analyte Benzene Bromobenzene 1,2-Dichlorobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene TestAmerica Tampa Analysis Batch: 660-87646 Result (ug/L) 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 0.15 0.50 Page 10 of 31 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 0.15 0.50 BVMH5973 1HK2026.D 5 mL 5 mL PQL 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 1.0 1.0 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: DMW-CC_111909 Lab Sample ID: Client Matrix: 660-32642-2 Water Job Number: 660-32642-1 Date Sampled: 11/19/2009 1715 Date Received: 11/20/2009 1045 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 11/20/2009 1917 11/20/2009 1917 Analysis Batch: 660-87646 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Analyte Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Result (ug/L) 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 Qualifier U U U U U U U U U U U U U U U J3 U U J3 U U Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane %Rec 100 97 92 Qualifier TestAmerica Tampa Page 11 of 31 MDL 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 BVMH5973 1HK2026.D 5 mL 5 mL PQL 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 70 - 130 70 - 130 70 - 130 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-32642-1 Client Sample ID: Trip Blank#4_111909 Lab Sample ID: Client Matrix: 660-32642-3 Water Date Sampled: 11/19/2009 0000 Date Received: 11/20/2009 1045 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 11/20/2009 1748 11/20/2009 1748 Analyte Benzene Bromobenzene 1,2-Dichlorobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene TestAmerica Tampa Analysis Batch: 660-87646 Result (ug/L) 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 0.15 0.50 Page 12 of 31 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 0.15 0.50 BVMH5973 1HK2022.D 5 mL 5 mL PQL 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 1.0 1.0 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-32642-1 Client Sample ID: Trip Blank#4_111909 Lab Sample ID: Client Matrix: 660-32642-3 Water Date Sampled: 11/19/2009 0000 Date Received: 11/20/2009 1045 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 11/20/2009 1748 11/20/2009 1748 Analysis Batch: 660-87646 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Analyte Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Result (ug/L) 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 Qualifier U U U U U U U U U U U U U U U J3 U U J3 U U Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane %Rec 91 97 91 Qualifier TestAmerica Tampa Page 13 of 31 MDL 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 BVMH5973 1HK2022.D 5 mL 5 mL PQL 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 70 - 130 70 - 130 70 - 130 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IMW-V_111909 Lab Sample ID: Client Matrix: 660-32642-1 Water Job Number: 660-32642-1 Date Sampled: 11/19/2009 1638 Date Received: 11/20/2009 1045 8260C _SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C _SIM/ID 5030C 1.0 11/20/2009 1832 11/20/2009 1832 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-87653 Result (ug/L) 5.7 Page 14 of 31 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier MDL 1.0 BVMH5973 1HK2024.D 5 mL 5 mL PQL 2.0 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-32642-1 Client Sample ID: DMW-CC_111909 Lab Sample ID: Client Matrix: 660-32642-2 Water Date Sampled: 11/19/2009 1715 Date Received: 11/20/2009 1045 8260C _SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C _SIM/ID 5030C 1.0 11/20/2009 1917 11/20/2009 1917 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-87653 Result (ug/L) 1.0 Page 15 of 31 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier U MDL 1.0 BVMH5973 1HK2026.D 5 mL 5 mL PQL 2.0 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-32642-1 Client Sample ID: Trip Blank#4_111909 Lab Sample ID: Client Matrix: 660-32642-3 Water Date Sampled: 11/19/2009 0000 Date Received: 11/20/2009 1045 8260C _SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C _SIM/ID 5030C 1.0 11/20/2009 1748 11/20/2009 1748 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-87653 Result (ug/L) 1.0 Page 16 of 31 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier U MDL 1.0 BVMH5973 1HK2022.D 5 mL 5 mL PQL 2.0 DATA REPORTING QUALIFIERS Client: ARCADIS U.S., Inc. Lab Section Job Number: 660-32642-1 Qualifier Description J3 Estimated value; value may not be accurate. Spike recovery or RPD outside of criteria. U Indicates that the compound was analyzed for but not detected. L Off-scale high. Actual value is known to be greater than the value given. I The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. GC/MS VOA TestAmerica Tampa Page 17 of 31 QUALITY CONTROL RESULTS TestAmerica Tampa Page 18 of 31 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-32642-1 Surrogate Recovery Report 8260B Volatile Organic Compounds (GC/MS) Client Matrix: Water TOL %Rec BFB %Rec DBFM %Rec Lab Sample ID Client Sample ID 660-32642-1 IMW-V_111909 111 95 93 660-32642-2 DMW-CC_111909 100 97 92 660-32642-3 Trip Blank#4_111909 91 97 91 MB 660-87646/4 108 97 93 LCS 660-87646/3 110 97 93 111 95 94 108 98 94 660-32564-C-11 MS 660-32642-1 DU IMW-V_111909 DU Surrogate TOL = Toluene-d8 (Surr) BFB = 4-Bromofluorobenzene DBFM = Dibromofluoromethane Acceptance Limits 70-130 70-130 70-130 TestAmerica Tampa Page 19 of 31 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-32642-1 Method Blank - Batch: 660-87646 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-87646/4 Water 1.0 11/20/2009 1304 11/20/2009 1304 Method: 8260B Preparation: 5030B Analysis Batch: 660-87646 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HK2010.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL Benzene Bromobenzene 1,2-Dichlorobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 20 of 31 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-32642-1 Method Blank - Batch: 660-87646 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-87646/4 Water 1.0 11/20/2009 1304 11/20/2009 1304 Method: 8260B Preparation: 5030B Analysis Batch: 660-87646 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HK2010.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene 0.59 0.98 0.63 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 U U U U U U U U U U U U U U U U U U U U U U U U 0.59 0.98 0.63 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 1.0 2.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane % Rec Acceptance Limits 108 97 93 70 - 130 70 - 130 70 - 130 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 21 of 31 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-32642-1 Lab Control Sample - Batch: 660-87646 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: LCS 660-87646/3 Water 1.0 11/20/2009 1051 11/20/2009 1051 Method: 8260B Preparation: 5030B Analysis Batch: 660-87646 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HK2004.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Spike Amount Result % Rec. Limit Benzene Bromobenzene 1,2-Dichlorobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.1 21.0 21.5 20.6 22.8 19.1 19.2 21.7 22.7 21.9 20.8 21.3 13.8 20.3 18.0 20.8 21.3 22.2 19.6 23.0 23.2 21.1 20.4 11.9 20.7 20.1 22.1 20.9 21.4 23.3 23.8 21.1 21.7 26.1 20.9 21.3 22.4 20.3 21.9 20.4 22.0 100 105 107 103 114 95 96 108 113 110 104 107 69 102 90 104 107 111 98 115 116 106 102 60 103 101 111 104 107 116 119 105 108 130 104 106 112 101 109 102 110 64 - 140 68 - 130 70 - 130 59 - 130 70 - 130 65 - 130 14 - 184 59 - 133 68 - 134 64 - 130 53 - 145 70 - 130 39 - 174 59 - 130 35 - 153 70 - 130 70 - 130 70 - 130 52 - 130 65 - 130 70 - 130 68 - 130 70 - 130 16 - 149 60 - 132 70 - 130 51 - 157 61 - 130 55 - 145 70 - 130 70 - 130 49 - 139 58 - 146 70 - 130 62 - 130 69 - 131 62 - 155 60 - 131 65 - 134 57 - 130 41 - 157 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 22 of 31 Qual Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-32642-1 Lab Control Sample - Batch: 660-87646 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: LCS 660-87646/3 Water 1.0 11/20/2009 1051 11/20/2009 1051 Method: 8260B Preparation: 5030B Analysis Batch: 660-87646 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HK2004.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Spike Amount Result % Rec. Limit N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 100 100 100 10.0 100 10.0 21.8 22.1 21.0 21.1 24.1 23.0 20.1 21.5 20.4 23.5 21.8 19.7 21.2 21.9 21.4 17.9 21.6 122 131 154 12.7 149 11.5 109 111 105 105 120 115 100 107 102 118 109 99 106 109 107 89 108 122 131 154 127 149 115 66 - 130 62 - 136 70 - 130 67 - 130 47 - 143 70 - 131 46 - 148 54 - 136 57 - 135 69 - 130 59 - 142 62 - 147 62 - 130 66 - 138 65 - 134 48 - 147 66 - 133 62 - 142 63 - 140 64 - 137 30 - 184 57 - 148 67 - 130 Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane % Rec Acceptance Limits 110 97 93 70 - 130 70 - 130 70 - 130 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 23 of 31 Qual J3 J3 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-32642-1 Matrix Spike - Batch: 660-87646 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-32564-C-11 MS Water 1.0 11/20/2009 1703 11/20/2009 1703 Method: 8260B Preparation: 5030B Analysis Batch: 660-87646 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HK2020.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Sample Result/Qual Spike Amount Result % Rec. Benzene Bromobenzene 1,2-Dichlorobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 21.4 21.2 21.3 20.5 23.2 18.0 10.6 21.9 23.6 22.7 22.9 22.1 15.9 21.4 18.1 21.6 21.7 22.3 18.0 23.0 23.8 21.5 20.6 12.6 22.2 21.2 24.5 22.4 23.0 24.5 24.5 22.3 23.8 26.4 20.4 22.4 107 106 106 102 116 90 53 110 118 113 114 110 79 107 91 108 109 112 90 115 119 107 103 63 111 106 122 112 115 123 122 112 119 132 102 112 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 24 of 31 Limit 64 - 140 68 - 130 70 - 130 59 - 130 70 - 130 65 - 130 14 - 184 59 - 133 68 - 134 64 - 130 53 - 145 70 - 130 39 - 174 59 - 130 35 - 153 70 - 130 70 - 130 70 - 130 52 - 130 65 - 130 70 - 130 68 - 130 70 - 130 16 - 149 60 - 132 70 - 130 51 - 157 61 - 130 55 - 145 70 - 130 70 - 130 49 - 139 58 - 146 70 - 130 62 - 130 69 - 131 Qual J3 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-32642-1 Matrix Spike - Batch: 660-87646 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-32564-C-11 MS Water 1.0 11/20/2009 1703 11/20/2009 1703 Method: 8260B Preparation: 5030B Analysis Batch: 660-87646 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HK2020.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Sample Result/Qual Spike Amount Result % Rec. Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 100 100 100 10.0 100 10.0 20.8 21.1 22.1 20.1 20.1 22.7 22.8 21.3 20.8 25.1 24.7 18.4 19.5 22.3 23.9 21.7 22.1 20.4 21.7 22.2 19.5 22.6 122 129 159 13.3 150 11.7 104 105 111 101 101 114 114 106 104 125 124 92 98 111 119 109 111 102 108 111 97 113 122 129 159 133 150 117 U U U U U U U U U U U U U U U U U U U U U U U U U U U U Surrogate % Rec Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane 111 95 94 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 25 of 31 Acceptance Limits 70 - 130 70 - 130 70 - 130 Limit 62 - 155 60 - 131 65 - 134 57 - 130 41 - 157 66 - 130 62 - 136 70 - 130 67 - 130 47 - 143 70 - 131 46 - 148 54 - 136 57 - 135 69 - 130 59 - 142 62 - 147 62 - 130 66 - 138 65 - 134 48 - 147 66 - 133 62 - 142 63 - 140 64 - 137 30 - 184 57 - 148 67 - 130 Qual J3 J3 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-32642-1 Duplicate - Batch: 660-87646 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-32642-1 Water 1.0 11/20/2009 1854 11/20/2009 1854 Method: 8260B Preparation: 5030B Analysis Batch: 660-87646 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HK2025.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Sample Result/Qual Result RPD Limit Qual Benzene Bromobenzene 1,2-Dichlorobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 26 of 31 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-32642-1 Duplicate - Batch: 660-87646 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-32642-1 Water 1.0 11/20/2009 1854 11/20/2009 1854 Method: 8260B Preparation: 5030B Analysis Batch: 660-87646 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HK2025.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Sample Result/Qual Result RPD Limit Qual Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene 4.0 2.5 0.59 0.98 0.63 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.93 4.4 0.44 0.60 4.0 2.5 0.59 0.98 0.63 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.886 4.4 0.44 0.60 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC 5 NC NC NC 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 U U U U U U U U U U U U U U U U U U U U U U J3 I U J3 U U U U U U U U U U U U U U U U U U U U U U U U I U U U Surrogate % Rec Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane 108 98 94 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 27 of 31 Acceptance Limits 70 - 130 70 - 130 70 - 130 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-32642-1 Method Blank - Batch: 660-87653 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: Method: 8260C _SIM/ID Preparation: 5030C MB 660-87653/4 Water 1.0 11/20/2009 1304 11/20/2009 1304 Analysis Batch: 660-87653 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HK2010.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL 1,4-Dioxane 1.0 U 1.0 2.0 Lab Control Sample - Batch: 660-87653 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: LCS 660-87653/3 Water 1.0 11/20/2009 1158 11/20/2009 1158 Method: 8260C _SIM/ID Preparation: 5030C Analysis Batch: 660-87653 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HK2007.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Spike Amount Result % Rec. Limit 1,4-Dioxane 25.0 21.9 88 50 - 150 Matrix Spike - Batch: 660-87653 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-32643-C-2 MS Water 1.0 11/20/2009 2110 11/20/2009 2110 Method: 8260C _SIM/ID Preparation: 5030C Analysis Batch: 660-87653 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HK2031.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Sample Result/Qual Spike Amount Result % Rec. 1,4-Dioxane 130 25.0 159 103 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Qual Page 28 of 31 Limit 50 - 150 Qual L Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-32642-1 Duplicate - Batch: 660-87653 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-32642-1 Water 1.0 11/20/2009 1854 11/20/2009 1854 Method: 8260C _SIM/ID Preparation: 5030C Analysis Batch: 660-87653 Prep Batch: N/A Units: ug/L Instrument ID: BVMH GC/MS Lab File ID: 1HK2025.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Sample Result/Qual Result RPD Limit 1,4-Dioxane 5.7 5.93 4 50 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 29 of 31 Qual Page 30 of 31 Login Sample Receipt Check List Client: ARCADIS U.S., Inc. Job Number: 660-32642-1 Login Number: 32642 Creator: Harrison, Amanda List Number: 1 List Source: TestAmerica Tampa Question T / F/ NA Radioactivity either was not measured or, if measured, is at or below background The cooler's custody seal, if present, is intact. N/A The cooler or samples do not appear to have been compromised or tampered with. Samples were received on ice. Cooler Temperature is acceptable. True Cooler Temperature is recorded. COC is present. COC is filled out in ink and legible. COC is filled out with all pertinent information. There are no discrepancies between the sample IDs on the containers and the COC. Samples are received within Holding Time. Sample containers have legible labels. Containers are not broken or leaking. True True True False True Sample collection date/times are provided. Appropriate sample containers are used. Sample bottles are completely filled. There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs VOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter. If necessary, staff have been informed of any short hold time or quick TAT needs Multiphasic samples are not present. Samples do not require splitting or compositing. Is the Field Sampler's name present on COC? Sample Preservation Verified True True True True TestAmerica Tampa Comment True True True True True True True True True True True True Page 31 of 31 2.7 degrees C CU-07 only rec'd 1 vial for Trip Blank 11.19.09 ANALYTICAL REPORT Job Number: 660-32804-1 Job Description: Raytheon For: ARCADIS U.S., Inc. 14055 Riveredge Drive Suite 400 Tampa, FL 33637 Attention: Mr. Gus Suarez _____________________________________________ Approved for release. Natalie Tafuni Project Manager I 12/8/2009 2:05 PM Natalie Tafuni Project Manager I [email protected] 12/08/2009 cc: Ms. Lyndi Mott Mr. Melvin Rivera Albert Zumbuhl Methods: FDEP, DOH Certification #: TestAmerica Tampa E84282 These test results meet all the requirements of NELAC unless specified in the case narrative. All questions regarding this test report should be directed to the TestAmerica Project Manager who signed this test report. The estimated uncertainty associated with these reported results is available upon request. The results contained in this test report relate only to these samples included herein. TestAmerica Laboratories, Inc. TestAmerica Tampa 6712 Benjamin Road, Suite 100, Tampa, FL 33634 Tel (813) 885-7427 Fax (813) 885-7049 www.testamericainc.com Page 1 of 28 Job Narrative 660-32804-1 Comments No additional comments. Receipt All samples were received in good condition within temperature requirements. 8260B The laboratory control sample (LCS) for batch 660-88145 was outside of control limits for MTBE. MTBE recovered high with samples non-detect for MTBE. The data are flagged with J3 qualifiers. The batch matrix spike (MS) recoveries for batch 660-88145(660-32795) were outside of control limits. The associated laboratory control sample (LCS) recovery met acceptance criteria except as noted above. The data are flagged with J3 qualifiers. The batch sample duplicate %RPD for batch 660-88145(660-32794) has a result of NC for most compounds. The sample result and the sample duplicate result are both Non-detect for these compounds. The Laboratory LIMs system flags the %RPD in this scenario as NC, or "not calculated". Page 2 of 28 EXECUTIVE SUMMARY - Detections Client: ARCADIS U.S., Inc. Lab Sample ID Analyte 660-32804-1 1,4-Dioxane Job Number: 660-32804-1 Client Sample ID Result / Qualifier Reporting Limit Units Method ug/L 8260C _SIM/ID IMW-V_120209 4.0 2.0 TestAmerica Tampa Page 3 of 28 METHOD SUMMARY Client: ARCADIS U.S., Inc. Description Job Number: 660-32804-1 Lab Location Method Preparation Method Volatile Organic Compounds (GC/MS) Purge and Trap TAL TAM TAL TAM SW846 8260B SW846 5030B 1,4-Dioxane by SIM/Isotopic Dilution Purge and Trap TAL TAM TAL TAM SW846 8260C _SIM/ID SW846 5030C Matrix Water Lab References: TAL TAM = TestAmerica Tampa Method References: SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. TestAmerica Tampa Page 4 of 28 METHOD / ANALYST SUMMARY Client: ARCADIS U.S., Inc. Job Number: 660-32804-1 Method Analyst SW846 8260B Harris, Chris CH SW846 8260C _SIM/ID Harris, Chris CH TestAmerica Tampa Page 5 of 28 Analyst ID SAMPLE SUMMARY Client: ARCADIS U.S., Inc. Job Number: 660-32804-1 Lab Sample ID Client Sample ID Client Matrix 660-32804-1 660-32804-2 IMW-V_120209 Trip Blank_120209 Water Water TestAmerica Tampa Page 6 of 28 Date/Time Sampled Date/Time Received 12/02/2009 1030 12/02/2009 0000 12/03/2009 1420 12/03/2009 1420 SAMPLE RESULTS TestAmerica Tampa Page 7 of 28 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IMW-V_120209 Lab Sample ID: Client Matrix: 660-32804-1 Water Job Number: 660-32804-1 Date Sampled: 12/02/2009 1030 Date Received: 12/03/2009 1420 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 12/04/2009 1738 12/04/2009 1738 Analyte Benzene Bromobenzene 1,2-Dichlorobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene TestAmerica Tampa Analysis Batch: 660-88145 Result (ug/L) 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 0.15 0.50 Page 8 of 28 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 0.15 0.50 BVMJ5975 1JL0423.D 5 mL 5 mL PQL 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 1.0 1.0 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IMW-V_120209 Lab Sample ID: Client Matrix: 660-32804-1 Water Job Number: 660-32804-1 Date Sampled: 12/02/2009 1030 Date Received: 12/03/2009 1420 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 12/04/2009 1738 12/04/2009 1738 Analysis Batch: 660-88145 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Analyte Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Result (ug/L) 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 Qualifier U U U U U U U U U U U U U U U U U U J3 U Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane %Rec 94 95 102 Qualifier TestAmerica Tampa Page 9 of 28 MDL 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 BVMJ5975 1JL0423.D 5 mL 5 mL PQL 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 70 - 130 70 - 130 70 - 130 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: Trip Blank_120209 Lab Sample ID: Client Matrix: 660-32804-2 Water Job Number: 660-32804-1 Date Sampled: 12/02/2009 0000 Date Received: 12/03/2009 1420 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 12/04/2009 1410 12/04/2009 1410 Analyte Benzene Bromobenzene 1,2-Dichlorobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene TestAmerica Tampa Analysis Batch: 660-88145 Result (ug/L) 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 0.15 0.50 Page 10 of 28 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MDL 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 0.15 0.50 BVMJ5975 1JL0414.D 5 mL 5 mL PQL 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 1.0 2.0 1.0 1.0 1.0 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: Trip Blank_120209 Lab Sample ID: Client Matrix: 660-32804-2 Water Job Number: 660-32804-1 Date Sampled: 12/02/2009 0000 Date Received: 12/03/2009 1420 8260B Volatile Organic Compounds (GC/MS) Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260B 5030B 1.0 12/04/2009 1410 12/04/2009 1410 Analysis Batch: 660-88145 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Analyte Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene Result (ug/L) 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 Qualifier U U U U U U U U U U U U U U U U U U J3 U Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane %Rec 94 97 100 Qualifier TestAmerica Tampa Page 11 of 28 MDL 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 BVMJ5975 1JL0414.D 5 mL 5 mL PQL 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Acceptance Limits 70 - 130 70 - 130 70 - 130 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IMW-V_120209 Lab Sample ID: Client Matrix: 660-32804-1 Water Job Number: 660-32804-1 Date Sampled: 12/02/2009 1030 Date Received: 12/03/2009 1420 8260C _SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C _SIM/ID 5030C 1.0 12/04/2009 1738 12/04/2009 1738 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-88144 Result (ug/L) 4.0 Page 12 of 28 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier MDL 1.0 BVMJ5975 1JL0423.D 5 mL 5 mL PQL 2.0 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-32804-1 Client Sample ID: Trip Blank_120209 Lab Sample ID: Client Matrix: 660-32804-2 Water Date Sampled: 12/02/2009 0000 Date Received: 12/03/2009 1420 8260C _SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C _SIM/ID 5030C 1.0 12/04/2009 1410 12/04/2009 1410 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-88144 Result (ug/L) 1.0 Page 13 of 28 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier U MDL 1.0 BVMJ5975 1JL0414.D 5 mL 5 mL PQL 2.0 DATA REPORTING QUALIFIERS Client: ARCADIS U.S., Inc. Lab Section Job Number: 660-32804-1 Qualifier Description J3 Estimated value; value may not be accurate. Spike recovery or RPD outside of criteria. U Indicates that the compound was analyzed for but not detected. I The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. GC/MS VOA TestAmerica Tampa Page 14 of 28 QUALITY CONTROL RESULTS TestAmerica Tampa Page 15 of 28 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-32804-1 Surrogate Recovery Report 8260B Volatile Organic Compounds (GC/MS) Client Matrix: Water Lab Sample ID Client Sample ID TOL %Rec BFB %Rec DBFM %Rec 660-32804-1 IMW-V_120209 94 95 102 660-32804-2 Trip Blank_120209 94 97 100 MB 660-88145/3 94 97 101 LCS 660-88145/2 97 93 108 660-32795-A-5 MS 97 95 104 660-32794-A-1 DU 95 98 101 Surrogate TOL = Toluene-d8 (Surr) BFB = 4-Bromofluorobenzene DBFM = Dibromofluoromethane Acceptance Limits 70-130 70-130 70-130 TestAmerica Tampa Page 16 of 28 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-32804-1 Method Blank - Batch: 660-88145 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-88145/3 Water 1.0 12/04/2009 1258 12/04/2009 1258 Method: 8260B Preparation: 5030B Analysis Batch: 660-88145 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JL0411.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL Benzene Bromobenzene 1,2-Dichlorobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 0.52 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 0.40 0.19 0.69 4.0 2.5 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 4.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 5.0 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 17 of 28 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-32804-1 Method Blank - Batch: 660-88145 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: MB 660-88145/3 Water 1.0 12/04/2009 1258 12/04/2009 1258 Method: 8260B Preparation: 5030B Analysis Batch: 660-88145 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JL0411.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene 0.59 0.98 0.63 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 U U U U U U U U U U U U U U U U U U U U U U U U 0.59 0.98 0.63 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.50 2.5 0.18 0.86 0.54 0.50 0.50 9.9 8.4 3.8 0.85 4.4 0.44 0.60 1.0 2.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 20 10 10 1.0 10 1.0 2.0 Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane % Rec Acceptance Limits 94 97 101 70 - 130 70 - 130 70 - 130 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 18 of 28 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-32804-1 Lab Control Sample - Batch: 660-88145 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: LCS 660-88145/2 Water 1.0 12/04/2009 1151 12/04/2009 1151 Method: 8260B Preparation: 5030B Analysis Batch: 660-88145 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JL0408.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Spike Amount Result % Rec. Limit Benzene Bromobenzene 1,2-Dichlorobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.4 18.8 18.8 20.5 22.2 18.5 27.2 17.0 17.3 16.3 21.4 18.9 18.8 20.4 18.3 17.3 16.8 23.0 17.3 21.1 20.2 18.3 18.0 18.8 20.2 21.5 17.7 19.7 20.1 19.8 19.9 20.3 21.6 21.2 20.3 18.7 22.5 16.5 17.5 20.8 18.8 102 94 94 102 111 93 136 85 87 81 107 94 94 102 91 87 84 115 87 105 101 92 90 94 101 108 88 98 101 99 100 101 108 106 102 93 113 82 87 104 94 64 - 140 68 - 130 70 - 130 59 - 130 70 - 130 65 - 130 14 - 184 59 - 133 68 - 134 64 - 130 53 - 145 70 - 130 39 - 174 59 - 130 35 - 153 70 - 130 70 - 130 70 - 130 52 - 130 65 - 130 70 - 130 68 - 130 70 - 130 16 - 149 60 - 132 70 - 130 51 - 157 61 - 130 55 - 145 70 - 130 70 - 130 49 - 139 58 - 146 70 - 130 62 - 130 69 - 131 62 - 155 60 - 131 65 - 134 57 - 130 41 - 157 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 19 of 28 Qual Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-32804-1 Lab Control Sample - Batch: 660-88145 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: LCS 660-88145/2 Water 1.0 12/04/2009 1151 12/04/2009 1151 Method: 8260B Preparation: 5030B Analysis Batch: 660-88145 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JL0408.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Spike Amount Result % Rec. Limit Qual N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 100 100 100 10.0 100 10.0 17.4 18.0 20.6 18.1 19.9 17.6 19.7 18.6 22.3 21.3 23.1 26.2 17.4 18.2 17.5 23.2 18.3 113 128 119 11.4 127 13.8 87 90 103 90 100 88 98 93 112 106 116 131 87 91 88 116 92 113 128 119 114 127 138 66 - 130 62 - 136 70 - 130 67 - 130 47 - 143 70 - 131 46 - 148 54 - 136 57 - 135 69 - 130 59 - 142 62 - 147 62 - 130 66 - 138 65 - 134 48 - 147 66 - 133 62 - 142 63 - 140 64 - 137 30 - 184 57 - 148 67 - 130 J3 Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane % Rec Acceptance Limits 97 93 108 70 - 130 70 - 130 70 - 130 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 20 of 28 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-32804-1 Matrix Spike - Batch: 660-88145 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-32795-A-5 MS Water 1.0 12/04/2009 2021 12/04/2009 2021 Method: 8260B Preparation: 5030B Analysis Batch: 660-88145 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JL0430.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Sample Result/Qual Spike Amount Result % Rec. Benzene Bromobenzene 1,2-Dichlorobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene 0.50 0.58 0.44 0.58 0.35 0.58 2.5 0.67 0.63 0.84 0.42 0.63 2.5 0.90 1.0 0.65 0.52 0.34 2.5 0.50 0.41 0.64 0.52 2.5 10 0.57 0.45 0.65 0.44 0.52 0.39 0.36 0.31 0.14 0.14 0.44 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 21.0 19.0 18.6 23.1 23.1 20.4 28.3 14.5 15.6 16.2 21.9 18.5 16.8 21.3 22.9 17.0 14.6 24.6 20.0 23.5 21.6 18.0 17.1 14.2 29.7 22.3 15.7 21.2 19.0 22.3 21.4 19.6 20.2 20.6 18.7 16.2 105 95 93 115 116 102 142 73 78 81 110 93 84 106 114 85 73 123 100 118 108 90 86 71 97 111 78 106 95 111 107 98 101 103 94 81 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 21 of 28 Limit 64 - 140 68 - 130 70 - 130 59 - 130 70 - 130 65 - 130 14 - 184 59 - 133 68 - 134 64 - 130 53 - 145 70 - 130 39 - 174 59 - 130 35 - 153 70 - 130 70 - 130 70 - 130 52 - 130 65 - 130 70 - 130 68 - 130 70 - 130 16 - 149 60 - 132 70 - 130 51 - 157 61 - 130 55 - 145 70 - 130 70 - 130 49 - 139 58 - 146 70 - 130 62 - 130 69 - 131 Qual Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-32804-1 Matrix Spike - Batch: 660-88145 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-32795-A-5 MS Water 1.0 12/04/2009 2021 12/04/2009 2021 Method: 8260B Preparation: 5030B Analysis Batch: 660-88145 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JL0430.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Sample Result/Qual Spike Amount Result % Rec. Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether 0.40 0.19 0.69 4.0 2.5 0.59 0.98 0.63 0.15 0.50 0.51 0.77 0.58 0.46 0.47 0.65 2.5 0.18 0.86 0.54 0.50 0.50 37 8.4 3.8 0.85 4.4 0.44 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 100 100 100 10.0 100 10.0 20.2 14.6 12.7 19.4 3.43 15.8 4.12 20.7 20.3 20.5 16.7 19.0 16.3 22.2 23.8 24.3 27.7 21.1 3.46 6.15 22.2 12.7 179 151 152 11.1 160 14.4 101 73 64 97 17 79 21 103 101 103 83 95 82 111 119 118 138 106 17 31 111 63 142 151 152 111 160 144 U U U U U U U U U U U U U U U I U U U U U U U U U U U Surrogate % Rec Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane 97 95 104 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 22 of 28 Acceptance Limits 70 - 130 70 - 130 70 - 130 Limit 62 - 155 60 - 131 65 - 134 57 - 130 41 - 157 66 - 130 62 - 136 70 - 130 67 - 130 47 - 143 70 - 131 46 - 148 54 - 136 57 - 135 69 - 130 59 - 142 62 - 147 62 - 130 66 - 138 65 - 134 48 - 147 66 - 133 62 - 142 63 - 140 64 - 137 30 - 184 57 - 148 67 - 130 Qual J3 I J3 J3 J3 J3 J3 J3 J3 J3 J3 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-32804-1 Duplicate - Batch: 660-88145 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-32794-A-1 DU Water 10 12/04/2009 1822 12/04/2009 1822 Method: 8260B Preparation: 5030B Analysis Batch: 660-88145 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JL0425.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Sample Result/Qual Result RPD Limit Qual Benzene Bromobenzene 1,2-Dichlorobenzene Chlorobromomethane Dichlorobromomethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Chlorodibromomethane 1,2-Dibromo-3-Chloropropane Ethylene Dibromide Dibromomethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene Isopropylbenzene 4-Isopropyltoluene 5.0 5.8 4.4 5.8 3.5 5.8 25 6.7 6.3 8.4 4.2 6.3 25 9.0 10 6.5 5.2 3.4 25 5.0 4.1 6.4 5.2 25 23 5.7 19 200 4.4 5.2 3.9 3.6 3.1 1.4 1.4 4.4 4.0 1.9 6.9 5.0 5.8 4.4 5.8 3.5 5.8 25 6.7 6.3 8.4 4.2 6.3 25 9.0 10 6.5 5.2 3.4 25 5.0 4.1 6.4 5.2 25 21.2 5.7 17.1 191 4.4 5.2 3.9 3.6 3.1 1.4 1.4 4.4 4.0 1.9 6.9 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC 7 NC 12 4 NC NC NC NC NC NC NC NC NC NC NC 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 23 of 28 U U U U U U U U U U U U Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-32804-1 Duplicate - Batch: 660-88145 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-32794-A-1 DU Water 10 12/04/2009 1822 12/04/2009 1822 Method: 8260B Preparation: 5030B Analysis Batch: 660-88145 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JL0425.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Sample Result/Qual Result RPD Limit Qual Methylene Chloride Naphthalene N-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene Acetone 2-Butanone (MEK) 4-Methyl-2-pentanone (MIBK) Carbon disulfide 2-Hexanone Methyl tert-butyl ether m-Xylene & p-Xylene 40 25 5.9 9.8 6.3 1.5 5.0 5.1 7.7 5.8 4.6 4.7 1400 25 1.8 8.6 5.4 17 5.0 99 84 38 8.5 44 4.4 6.0 40 25 5.9 9.8 6.3 1.5 5.0 5.1 7.7 5.8 4.6 4.7 1320 25 1.8 8.6 5.4 15.8 5.0 99 84 38 8.5 44 4.4 6.0 NC NC NC NC NC NC NC NC NC NC NC NC 5 NC NC NC NC 5 NC NC NC NC NC NC NC NC 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 30 U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U Surrogate % Rec Toluene-d8 (Surr) 4-Bromofluorobenzene Dibromofluoromethane 95 98 101 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 24 of 28 Acceptance Limits 70 - 130 70 - 130 70 - 130 U U U U U U U U U U U J3 U Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-32804-1 Method Blank - Batch: 660-88144 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: Method: 8260C _SIM/ID Preparation: 5030C MB 660-88144/4 Water 1.0 12/04/2009 1258 12/04/2009 1258 Analysis Batch: 660-88144 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JL0411.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL 1,4-Dioxane 1.0 U 1.0 2.0 Lab Control Sample - Batch: 660-88144 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: LCS 660-88144/3 Water 1.0 12/04/2009 1044 12/04/2009 1044 Method: 8260C _SIM/ID Preparation: 5030C Analysis Batch: 660-88144 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JL0405.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Spike Amount Result % Rec. Limit 1,4-Dioxane 25.0 22.3 89 50 - 150 Matrix Spike - Batch: 660-88144 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-32795-A-5 MS Water 1.0 12/04/2009 1956 12/04/2009 1956 Method: 8260C _SIM/ID Preparation: 5030C Analysis Batch: 660-88144 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JL0429.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Sample Result/Qual Spike Amount Result % Rec. 1,4-Dioxane 1.0 25.0 22.9 92 U Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Qual Page 25 of 28 Limit 50 - 150 Qual Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-32804-1 Duplicate - Batch: 660-88144 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-32794-A-1 DU Water 10 12/04/2009 1822 12/04/2009 1822 Method: 8260C _SIM/ID Preparation: 5030C Analysis Batch: 660-88144 Prep Batch: N/A Units: ug/L Instrument ID: BVMJ GC/MS Lab File ID: 1JL0425.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Sample Result/Qual Result RPD Limit 1,4-Dioxane 260 376 37 50 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 26 of 28 Qual Page 27 of 28 Login Sample Receipt Check List Client: ARCADIS U.S., Inc. Job Number: 660-32804-1 Login Number: 32804 Creator: Harrison, Amanda List Number: 1 List Source: TestAmerica Tampa Question T / F/ NA Radioactivity either was not measured or, if measured, is at or below background The cooler's custody seal, if present, is intact. N/A The cooler or samples do not appear to have been compromised or tampered with. Samples were received on ice. Cooler Temperature is acceptable. True Cooler Temperature is recorded. COC is present. COC is filled out in ink and legible. COC is filled out with all pertinent information. There are no discrepancies between the sample IDs on the containers and the COC. Samples are received within Holding Time. Sample containers have legible labels. Containers are not broken or leaking. True True True True True Sample collection date/times are provided. Appropriate sample containers are used. Sample bottles are completely filled. There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs VOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter. If necessary, staff have been informed of any short hold time or quick TAT needs Multiphasic samples are not present. Samples do not require splitting or compositing. Is the Field Sampler's name present on COC? Sample Preservation Verified True True True True TestAmerica Tampa Comment True True True True True True True True True True True True Page 28 of 28 3.0 degrees C CU-07 ANALYTICAL REPORT Job Number: 660-33568-1 Job Description: Raytheon For: ARCADIS U.S., Inc. 14055 Riveredge Drive Suite 400 Tampa, FL 33637 Attention: Mr. Gus Suarez _____________________________________________ Approved for release. Natalie Tafuni Project Manager I 2/1/2010 3:27 PM Natalie Tafuni Project Manager I [email protected] 02/01/2010 cc: Ms. Lyndi Mott Mr. Melvin Rivera Albert Zumbuhl Methods: FDEP, DOH Certification #: TestAmerica Tampa E84282 These test results meet all the requirements of NELAC unless specified in the case narrative. All questions regarding this test report should be directed to the TestAmerica Project Manager who signed this test report. The estimated uncertainty associated with these reported results is available upon request. The results contained in this test report relate only to these samples included herein. TestAmerica Laboratories, Inc. TestAmerica Tampa 6712 Benjamin Road, Suite 100, Tampa, FL 33634 Tel (813) 885-7427 Fax (813) 885-7049 www.testamericainc.com Page 1 of 17 Job Narrative 660-33568-1 Comments No additional comments. Receipt All samples were received in good condition within temperature requirements. Page 2 of 17 EXECUTIVE SUMMARY - Detections Client: ARCADIS U.S., Inc. Lab Sample ID Analyte 660-33568-1 Client Sample ID Result / Qualifier 1,4-Dioxane Units Method 4.9 2.0 ug/L 8260C _SIM/ID 2.1 2.0 ug/L 8260C _SIM/ID 58 2.0 ug/L 8260C _SIM/ID IMW-V_012910 1,4-Dioxane 660-33568-3 Reporting Limit IMW-21_012910 1,4-Dioxane 660-33568-2 Job Number: 660-33568-1 SMW-B_012910 TestAmerica Tampa Page 3 of 17 METHOD SUMMARY Client: ARCADIS U.S., Inc. Description Job Number: 660-33568-1 Lab Location Method Preparation Method Matrix: Water 1,4-Dioxane by SIM/Isotopic Dilution Purge and Trap TAL TAM TAL TAM SW846 8260C _SIM/ID SW846 5030C Lab References: TAL TAM = TestAmerica Tampa Method References: SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. TestAmerica Tampa Page 4 of 17 METHOD / ANALYST SUMMARY Client: ARCADIS U.S., Inc. Job Number: 660-33568-1 Method Analyst SW846 8260C _SIM/ID Harris, Chris TestAmerica Tampa Page 5 of 17 Analyst ID CH SAMPLE SUMMARY Client: ARCADIS U.S., Inc. Job Number: 660-33568-1 Lab Sample ID Client Sample ID Client Matrix 660-33568-1 660-33568-2 660-33568-3 660-33568-4 IMW-21_012910 IMW-V_012910 SMW-B_012910 Trip Blank_012910 Water Water Water Water TestAmerica Tampa Page 6 of 17 Date/Time Sampled 01/29/2010 01/29/2010 01/29/2010 01/29/2010 1008 1119 1230 1008 Date/Time Received 01/29/2010 01/29/2010 01/29/2010 01/29/2010 1315 1315 1315 1315 SAMPLE RESULTS TestAmerica Tampa Page 7 of 17 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-33568-1 Client Sample ID: IMW-21_012910 Lab Sample ID: Client Matrix: 660-33568-1 Water Date Sampled: 01/29/2010 1008 Date Received: 01/29/2010 1315 8260C _SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C _SIM/ID 5030C 1.0 02/01/2010 1221 02/01/2010 1221 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-90107 Result (ug/L) 4.9 Page 8 of 17 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier MDL 1.0 BVMM5971 1MB0109.D 5 mL 5 mL PQL 2.0 Analytical Data Client: ARCADIS U.S., Inc. Client Sample ID: IMW-V_012910 Lab Sample ID: Client Matrix: 660-33568-2 Water Job Number: 660-33568-1 Date Sampled: 01/29/2010 1119 Date Received: 01/29/2010 1315 8260C _SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C _SIM/ID 5030C 1.0 02/01/2010 1240 02/01/2010 1240 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-90107 Result (ug/L) 2.1 Page 9 of 17 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier MDL 1.0 BVMM5971 1MB0110.D 5 mL 5 mL PQL 2.0 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-33568-1 Client Sample ID: SMW-B_012910 Lab Sample ID: Client Matrix: 660-33568-3 Water Date Sampled: 01/29/2010 1230 Date Received: 01/29/2010 1315 8260C _SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C _SIM/ID 5030C 1.0 02/01/2010 1301 02/01/2010 1301 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-90107 Result (ug/L) 58 Page 10 of 17 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier MDL 1.0 BVMM5971 1MB0111.D 5 mL 5 mL PQL 2.0 Analytical Data Client: ARCADIS U.S., Inc. Job Number: 660-33568-1 Client Sample ID: Trip Blank_012910 Lab Sample ID: Client Matrix: 660-33568-4 Water Date Sampled: 01/29/2010 1008 Date Received: 01/29/2010 1315 8260C _SIM/ID 1,4-Dioxane by SIM/Isotopic Dilution Method: Preparation: Dilution: Date Analyzed: Date Prepared: 8260C _SIM/ID 5030C 1.0 02/01/2010 1103 02/01/2010 1103 Analyte 1,4-Dioxane TestAmerica Tampa Analysis Batch: 660-90107 Result (ug/L) 1.0 Page 11 of 17 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Qualifier U MDL 1.0 BVMM5971 1MB0108.D 5 mL 5 mL PQL 2.0 DATA REPORTING QUALIFIERS Client: ARCADIS U.S., Inc. Lab Section Job Number: 660-33568-1 Qualifier Description U Indicates that the compound was analyzed for but not detected. GC/MS VOA TestAmerica Tampa Page 12 of 17 QUALITY CONTROL RESULTS TestAmerica Tampa Page 13 of 17 Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-33568-1 Method Blank - Batch: 660-90107 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: Method: 8260C _SIM/ID Preparation: 5030C MB 660-90107/2 Water 1.0 02/01/2010 1026 02/01/2010 1026 Analysis Batch: 660-90107 Prep Batch: N/A Units: ug/L Instrument ID: 5971 GC/MS Lab File ID: 1MB0106.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Result Qual MDL PQL 1,4-Dioxane 1.0 U 1.0 2.0 Lab Control Sample - Batch: 660-90107 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: LCS 660-90107/1 Water 1.0 02/01/2010 0947 02/01/2010 0947 Method: 8260C _SIM/ID Preparation: 5030C Analysis Batch: 660-90107 Prep Batch: N/A Units: ug/L Instrument ID: 5971 GC/MS Lab File ID: 1MB0104.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Spike Amount Result % Rec. Limit 1,4-Dioxane 25.0 26.8 107 50 - 150 Matrix Spike - Batch: 660-90107 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-33568-1 Water 1.0 02/01/2010 1338 02/01/2010 1338 Method: 8260C _SIM/ID Preparation: 5030C Analysis Batch: 660-90107 Prep Batch: N/A Units: ug/L Instrument ID: 5971 GC/MS Lab File ID: 1MB0113.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Sample Result/Qual Spike Amount Result % Rec. 1,4-Dioxane 4.9 25.0 30.1 101 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Qual Page 14 of 17 Limit 50 - 150 Qual Quality Control Results Client: ARCADIS U.S., Inc. Job Number: 660-33568-1 Duplicate - Batch: 660-90107 Lab Sample ID: Client Matrix: Dilution: Date Analyzed: Date Prepared: 660-33568-1 Water 1.0 02/01/2010 1319 02/01/2010 1319 Method: 8260C _SIM/ID Preparation: 5030C Analysis Batch: 660-90107 Prep Batch: N/A Units: ug/L Instrument ID: 5971 GC/MS Lab File ID: 1MB0112.D Initial Weight/Volume: 5 mL Final Weight/Volume: 5 mL Analyte Sample Result/Qual Result RPD Limit 1,4-Dioxane 4.9 8.00 48 50 Calculations are performed before rounding to avoid round-off errors in calculated results. TestAmerica Tampa Page 15 of 17 Qual Page 16 of 17 Login Sample Receipt Check List Client: ARCADIS U.S., Inc. Job Number: 660-33568-1 Login Number: 33568 Creator: Volz, Charles List Number: 1 List Source: TestAmerica Tampa Question T / F/ NA Radioactivity either was not measured or, if measured, is at or below background The cooler's custody seal, if present, is intact. The cooler or samples do not appear to have been compromised or tampered with. Samples were received on ice. Cooler Temperature is acceptable. Cooler Temperature is recorded. COC is present. COC is filled out in ink and legible. COC is filled out with all pertinent information. There are no discrepancies between the sample IDs on the containers and the COC. Samples are received within Holding Time. Sample containers have legible labels. Containers are not broken or leaking. Sample collection date/times are provided. Appropriate sample containers are used. Sample bottles are completely filled. There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs VOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter. If necessary, staff have been informed of any short hold time or quick TAT needs Multiphasic samples are not present. Samples do not require splitting or compositing. Is the Field Sampler's name present on COC? Sample Preservation Verified N/A Comment True True True True True True True True True True True True True True True True True True True True True True TestAmerica Tampa Page 17 of 17 4.3 Degrees C. CU-07